(5-Hydroxy-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl)(pyridin-4-yl)methanone monohydrate

被引：6
|
作者：
Kargar, Hadi [2 ]
Kia, Reza [1 ,3 ]
Froozandeh, Fatemeh [2 ]
Sadr, Moayad Hossaini [4 ]
Tahir, Muhammad Nawaz [5 ]
机构：
[1] Islamic Azad Univ, Dept Chem, Sci & Res Branch, Tehran, Iran
[2] PNU, Sch Sci, Dept Chem, Yazd, Iran
[3] Islamic Azad Univ, Xray Crystallog Lab, Plasma Phys Res Ctr, Sci & Res Branch, Tehran, Iran
[4] Azarbaijan Univ Tarbiat Moallem, Dept Chem, Tabriz, Iran
[5] Univ Sargodha, Dept Phys, Punjab, Pakistan
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
D O I：
10.1107/S160053681005275X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C16H15N3O2 center dot H2O, the mean plane of the approximately planar pyrazole ring [maximum deviation = 0.0474 (18) angstrom] makes dihedral angles of 86.32 (11) and 45.04 (10)degrees with the phenyl and pyridine rings, respectively. The dihedral angle between the phenyl and pyridine rings is 69.62 (11)degrees. In the crystal, intermolecular O-H center dot center dot center dot O and O-H center dot center dot center dot N hydrogen bonds connect the components into chains along [010]. The crystal structure is further stabilized by pi-pi stacking interactions with centroid-centroid distances of 3.7730 (12) angstrom.
引用
收藏
页码：O209 / U3199
页数：10
相关论文
共 50 条
  • [41] 1-[5-(4-Bromophenyl)-3-(4-fluorophenyl)-4,5-dihydro-1H-pyrazol-1-yl]-ethanone
    Fun, Hoong-Kun
    Loh, Wan-Sin
    Sapnakumari, M.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02586 - +
  • [42] Design, Synthesis, and Cytotoxicity Evaluation of 3-(5-(3-(aryl)-1-phenyl-1H-pyrazol-4-yl)-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)pyridine and 5-(3-(aryl)-1-phenyl-1H-pyrazol-4-yl)-3-(pyridin-3-yl)-4,5-dihydropyrazole-1-carbaldehyde Derivatives as Potential Anticancer Agents
    Alam, Raquib
    Alam, Md. Aftab
    Panda, Amulya K.
    Rahisuddin
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2017, 54 (03) : 1812 - 1821
  • [43] 3-Methyl-1-(pyridin-2-yl)-4-(1-pyridin-2-yl-3-methyl-1H-pyrazol-5-yl)-2H-3-pyrazolin-5(1H)-one
    Djerrari, B
    Essassi, EM
    Fifani, J
    Pierrot, M
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2001, 57 : O1126 - O1127
  • [44] 4-(3-Methyl-5-phenyl-1H-pyrazol-1-yl)benzenesulfonamide
    Asiri, Abdullah M.
    Faidallah, Hassan M.
    Al-Youbi, Abdulrahman O.
    Basaif, Salem A.
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2426 - U1104
  • [45] 4-[(4-Chlorophenyl)(5-hydroxy-3-methyl-1-phenyl-1H-pyrazol-4-yl) methyl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one
    Fun, Hoong-Kun
    Jebas, Samuel Robinson
    Girish, K. S.
    Kalluraya, B.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2301 - U1984
  • [46] Synthesis and Characterization of Novel 2-(1,2,3-Triazol-4-yl)-4,5-dihydro-1H-pyrazol-1-yl)thiazoles and 2-(4,5-Dihydro-1H-pyrazol-1-yl)-4-(1H-1,2,3-triazol-4-yl)thiazoles
    Kariuki, Benson M.
    Abdel-Wahab, Bakr F.
    Mohamed, Hanan A.
    Bekheit, Mohamed S.
    El-Hiti, Gamal A.
    MOLECULES, 2022, 27 (24):
  • [47] 1-[5-(Anthracen-9-yl)-3-(4-nitrophenyl)-4,5-dihydro-1H-pyrazol-1-yl]ethan-1-one
    Dong, Bao-Li
    Wang, Ming-Liang
    Li, Yong-Hua
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O386 - U817
  • [48] 4-{(2,4-Dichlorophenyl)[5-hydroxy-1-phenyl-3-(trifluoromethyl)-1H-pyrazol-4yl]methyl}-1-phenyl-3(trifluoromethyl)-1H-pyrazol-5-ol monohydrate
    Yao, CS
    Yu, CX
    Tu, SJ
    Wang, XS
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O771 - O773
  • [49] Efficient Synthesis of New Biheterocyclic 5-[(5-Trifluoromethyl-5-hydroxy-4,5-dihydro-1H-pyrazol-1-yl)-1-propan-1-one-3-yl]-2-methyl-7-trifluoromethylpyrazolo[1,5-a]pyrimidines
    Flores, Alex F. C.
    Rosales, Pauline F.
    Malavolta, Juliana L.
    Flores, Darlene C.
    JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2014, 25 (08) : 1439 - 1445
  • [50] 1-{3-(4-Methylphenyl)-5-[5-(2-nitrophenyl)furan-2-yl]-4,5-dihydro-1H-pyrazol-1-yl}ethanone
    Vinutha, N.
    Kumar, S. Madan
    Jois, B. S. Vidyashree
    Balakrishna, Kalluraya
    Lokanath, N. K.
    Revannasiddaiah, D.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1528 - +
12345