Determination of 93Zr and 237Np in nuclear power plant wastes

被引:18
|
作者
Osvath, Sz [1 ]
Vajda, N. [2 ]
Stefanka, Zs [3 ]
Szeles, E. [4 ]
Molnar, Zs [2 ]
机构
[1] Budapest Univ Technol & Econ, Inst Nucl Tech BME NTI, H-1111 Budapest, Hungary
[2] RadAnal Ltd, H-1121 Budapest, Hungary
[3] Hungarian Atom Energy Author OAH, H-1036 Budapest, Hungary
[4] Hungarian Acad Sci, Inst Isotopes MTA IKI, H-1121 Budapest, Hungary
关键词
Radiochemical analysis; Zirconium; Neptunium; UTEVA; ICP-MS; EXTRACTION CHROMATOGRAPHIC-SEPARATION; PLASMA-MASS SPECTROMETRY; ISOTOPE-DILUTION; ACTINIDES; HF;
D O I
10.1007/s10967-010-0886-9
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A combined radioanalytical method for determination of Zr-93 and Np-237 (as well as other actinoids) in radioactive wastes has been developed. Analytes were co-precipitated on iron(II)-hydroxide, separated and purified on UTEVA columns, and detected by inductively coupled plasma mass spectrometry. According to Zr and Np, 65 and 75% yields were achieved, respectively.
引用
收藏
页码:459 / 463
页数:5
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