Survey of T-2 and HT-2 toxins by LC-MS/MS in oats and oat products from European oat mills in 2005-2009

被引：38

作者：

Pettersson, Hans ^{[1
]}

Brown, Colin ^{[2
]}

Hauk, Julia ^{[2
]}

Hoth, Stefan ^{[2
]}

Meyer, Jens ^{[2
]}

Wessels, Detlev ^{[3
]}

机构：

[1] Swedish Univ Agr Sci, Dept Anim Nutr & Management, S-75007 Uppsala, Sweden

[2] European Breakfast Cereal Assoc, CEEREAL, B-1040 Brussels, Belgium

[3] Gesell Bioanalyt Hamburg mbH, D-21073 Hamburg, Germany

来源：

FOOD ADDITIVES & CONTAMINANTS PART B-SURVEILLANCE | 2011年 / 4卷 / 02期

关键词：

cereals; cereals and grain; mycotoxins; trichothecenes; fusarium toxins; oats; T-2; toxin; HT-2; milling; FUSARIUM TOXINS; NATURAL OCCURRENCE; HEAD BLIGHT; TRICHOTHECENES; CEREALS; GRAINS;

D O I：

10.1080/19393210.2011.561933

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

T-2 and HT-2 toxins were analysed in oats (n = 243), oat flakes (n = 529), oat meal (n = 105) and oat by-products (n = 209) from 11 European mills during 2005-2009 by high-performance liquid chromatography with a triple quadrupole mass spectrometer. Limits of quantification were 5 mu g kg-1 for both T-2 and HT-2 toxins in oats. The incidence of T-2 + HT-2 (5 mu g kg-1) in oats, oat flakes, oat meal and oat by-products was 93, 77, 34 and 99%, respectively. The mean values of T-2 + HT-2 were 94, 17, 11 and 293 mu g kg-1 for oats, oat flakes, oat meal and oat by-products, respectively. T-2 and HT-2 occurred together and the T-2 level was 52% of HT-2 in oats. Maximal T-2 and HT-2 concentration in oat flakes and oat meal were 197 and 118 mu g kg-1. The toxins were reduced by 82-88% during processing, but increased 3.1 times in oat by-products.

引用

页码：110 / 115

页数：6

共 50 条

[11] T-2 and HT-2 toxins in oats grown in Northern Europe
Pettersson, Hans
Borjesson, Thomas
Persson, Lars
Lerenius, Cecilia
Berg, Gunilla
Gustafsson, Goran
CEREAL RESEARCH COMMUNICATIONS, 2008, 36 : 591 - 592
[12] Analysis of Aflatoxins, Fumonisins, Deoxynivalenol, Ochratoxin A, Zearalenone, HT-2, and T-2 Toxins in Animal Feed by LC-MS/MS Using Cleanup with a Multi-Antibody Immunoaffinity Column
Mackay, Naomi
Marley, Elaine
Leeman, Dave
Poplawski, Cezary
Donnelly, Carol
JOURNAL OF AOAC INTERNATIONAL, 2022, 105 (05) : 1330 - 1340
[13] Efficacy of low pressure DBD plasma in the reduction of T-2 and HT-2 toxin in oat flour
Kis, Maja
Milosevic, Slobodan
Vulic, Ana
Herceg, Zoran
Vukusic, Tomislava
Pleadin, Jelka
FOOD CHEMISTRY, 2020, 316
[14] Development of a multicomponent method for Fusarium toxins using LC-MS/MS and its application during a survey for the content of T-2 toxin and deoxynivalenol in various feed and food samples
Biselli, S
Hummert, C
FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 2005, 22 (08): : 752 - 760
[15] T-2 and HT-2 toxins in harvested oat grains and their prevalence in whole grain flour during storage
Janaviciene, Sigita
Mankeviciene, Audrone
Kochiieru, Yuliia
Venslovas, Eimantas
FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 2022, 39 (07): : 1284 - 1295
[16] Simultaneous determination of aflatoxins, T-2 and HT-2 toxins, and fumonisins in cereal-derived products by QuEChERS extraction coupled with LC-MS/MS
Loredana Annunziata
Arianna Stramenga
Pierina Visciano
Maria Schirone
Lorenzo De Colli
Maria Novella Colagrande
Guido Campana
Giampiero Scortichini
Analytical and Bioanalytical Chemistry, 2017, 409 : 5143 - 5155
[17] Observation of T-2 Toxin and HT-2 Toxin Glucosides from Fusarium sporotrichioides by Liquid Chromatography Coupled to Tandem Mass Spectrometry (LC-MS/MS)
Busman, Mark
Poling, Stephen M.
Maragos, Chris M.
TOXINS, 2011, 3 (12) : 1554 - 1568
[18] Analysis of T-2 and HT-2 toxins in oats and other cereals by means of HPLC with fluorescence detection
Meister U.
Mycotoxin Research, 2008, 24 (1) : 31 - 39
[19] Development and validation of a reliable LC-MS/MS method for simultaneous determination of deoxynivalenol and T-2 toxin in maize and oats
Tahoun, Ibrahim F.
Gab-Allah, Mohamed A.
Yamani, Randa N.
Shehata, Adel B.
MICROCHEMICAL JOURNAL, 2021, 169
[20] Emerging issues of HT-2 and T-2 toxins in European cereal production
Edwards, S. G.
Barrier-Guillot, B.
Clasen, P-E.
Hietaniemi, V.
Pettersson, H.
WORLD MYCOTOXIN JOURNAL, 2009, 2 (02) : 173 - 179

← 1 2 3 4 5 →