Structural, optical, and antibacterial characteristics of mixed metal oxide CdO-NiO-Fe2O3 nanocomposites prepared using a self-combustion method at different polyvinyl alcohol concentrations

被引:11
作者
Al-Mushki, Asma A. A. [2 ]
Ahmed, Abdullah Ahmed Ali [1 ,2 ]
Abdulwahab, A. M. [2 ]
Al-Asbahi, Bandar Ali [3 ]
Abduljalil, Jameel M. A. [4 ]
Saad, Fuad A. A. [4 ]
Al-Hada, Naif M. [2 ,5 ]
Qaid, Saif M. H. [3 ]
Ghaithan, Hamid M. [3 ]
机构
[1] Univ Hamburg, Ctr Hybrid Nanostruct CHyN, D-20146 Hamburg, Germany
[2] Thamar Univ, Fac Sci Appl, Dept Phys, Dhamar 87246, Yemen
[3] King Saud Univ, Dept Phys & Astron, Coll Sci, POB 2455, Riyadh 11451, Saudi Arabia
[4] Thamar Univ, Fac Sci Appl, Dept Biol, Dhamar 87246, Yemen
[5] Dezhou Univ, Shandong Key Lab Biophys, Inst Biophys, Dezhou 253023, Peoples R China
来源
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING | 2022年 / 128卷 / 04期
关键词
CdO-NiO-Fe2O3; nanocomposites; Self-combustion method; PVA; Structural properties; Optical properties; Antibacterial activity; HETEROSTRUCTURED NANOCOMPOSITE; MORAXELLA-CATARRHALIS; IRON-OXIDE; NANOPARTICLES; FABRICATION; GAMMA-FE2O3; TOXICITY; PATHOGEN; BEHAVIOR; RESPECT;
D O I
10.1007/s00339-022-05428-w
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this study, the impact of polyvinyl alcohol (PVA) concentration on the sizes of mixed metal oxide (MMO) CdO-NiO-Fe2O3 nanocomposites was investigated. The results showed major improvements in the structural and optical properties that promote antibacterial activity. Self-combustion was used to synthesize MMO nanocomposites. X-ray diffraction (XRD), transmission electron microscopy (TEM), and Fourier-transform infrared (FTIR) spectroscopy were used to analyze the structural properties of the prepared samples. The optical properties of the MMO nanocomposites were examined using a UV-Visible spectrophotometer and photoluminescence (PL) spectroscopy. XRD analysis revealed a face-centred cubic structure for the CdO and NiO phases, whereas gamma-Fe2O3 had a cubic spinel crystalline structure. TEM analysis revealed that the size of the MMO nanocomposites increased from approximately 7.4-25.1 nm as the PVA concentration decreased from 0.05 to 0.0125 g/ml. Owing to the quantum confinement of MMO, the optical band gap values of the samples varied in relation to the PVA concentration. In this study, CdO-NiO-Fe2O3 nanocomposites were investigated for their antibacterial activities against Gram-positive bacteria (Staphylococcus aureus) and Gram-negative bacteria (Pseudomonas aeruginosa, Escherichia coli, and Moraxella catarrhalis). The results suggest that these materials are promising candidates for antibiotic applications.
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页数:15
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