Structural and Magnetic Properties of FePd Thin Film Synthesized by Electrodeposition Method

被引:11
作者
Barrera, Gabriele [1 ]
Scaglione, Federico [2 ,3 ]
Cialone, Matteo [2 ,3 ,4 ]
Celegato, Federica [1 ]
Coisson, Marco [1 ]
Rizzi, Paola [2 ,3 ]
Tiberto, Paola [1 ]
机构
[1] Ist Nazl Ric Metrol INRiM, Adv Mat Metrol & Life Sci, Str Cacce 91, I-10135 Turin, Italy
[2] Univ Turin, Dipartimento Chim, Via Pietro Giuria 7, I-10125 Turin, Italy
[3] Univ Turin, Ctr Interdipartimentale NIS Nanostruct Surfaces &, Via Pietro Giuria 7, I-10125 Turin, Italy
[4] Univ Autonoma Barcelona, Dept Fis, Cerdanyola Del Valles 08193, Spain
关键词
FePd alloy; electrodeposition technique; magnetic properties; structural characterisation; SURFACE-MORPHOLOGY; PD; WETTABILITY; REVERSAL; CATALYST; NANOWIRES; PALLADIUM; ALLOY; NI; MICROSTRUCTURE;
D O I
10.3390/ma13061454
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Bimetallic nanomaterials in the form of thin film constituted by magnetic and noble elements show promising properties in different application fields such as catalysts and magnetic driven applications. In order to tailor the chemical and physical properties of these alloys to meet the applications requirements, it is of great importance scientific interest to study the interplay between properties and morphology, surface properties, microstructure, spatial confinement and magnetic features. In this manuscript, FePd thin films are prepared by electrodeposition which is a versatile and widely used technique. Compositional, morphological, surface and magnetic properties are described as a function of deposition time (i.e., film thickness). Chemical etching in hydrochloric acid was used to enhance the surface roughness and help decoupling crystalline grains with direct consequences on to the magnetic properties. X-ray diffraction, SEM/AFM images, contact angle and magnetic measurements have been carried out with the aim of providing a comprehensive characterisation of the fundamental properties of these bimetallic thin films.
引用
收藏
页数:15
相关论文
共 52 条
[11]   THE PALLADIUM-HYDROGEN SYSTEM [J].
FLANAGAN, TB ;
OATES, WA .
ANNUAL REVIEW OF MATERIALS SCIENCE, 1991, 21 :269-304
[12]   Roughness dependent wettability of sputtered copper thin films: The effect of the local surface slope [J].
Foadi, Farnaz ;
ten Brink, Gert H. ;
Mohammadizadeh, Mohammad Reza ;
Palasantzas, George .
JOURNAL OF APPLIED PHYSICS, 2019, 125 (24)
[13]  
Gamburg YD, 2011, THEORY AND PRACTICE OF METAL ELECTRODEPOSITION, P1, DOI 10.1007/978-1-4419-9669-5
[14]   Studies on the synthesis, dealloying, and electrocatalytic properties of CoPd nanocatalysts [J].
Gan, Ya-Li ;
Yang, Yi ;
Du, Juan-Juan ;
Zhang, Rong-Hua ;
Dai, Zhong-Xu ;
Zhou, Xin-Wen .
JOURNAL OF SOLID STATE ELECTROCHEMISTRY, 2015, 19 (06) :1799-1805
[15]   Size and composition dependence in the optical properties of mixed (transition metal/noble metal) embedded clusters -: art. no. 155409 [J].
Gaudry, M ;
Cottancin, E ;
Pellarin, M ;
Lermé, J ;
Arnaud, L ;
Huntzinger, JR ;
Vialle, JL ;
Broyer, M ;
Rousset, JL ;
Treilleux, M ;
Mélinon, P .
PHYSICAL REVIEW B, 2003, 67 (15)
[16]   Review on noble metal-based catalysts for formaldehyde oxidation at room temperature [J].
Guo, Jiahong ;
Lin, Chuxia ;
Jiang, Chuanjia ;
Zhang, Pengyi .
APPLIED SURFACE SCIENCE, 2019, 475 :237-255
[17]   Electrodeposition of Fe70Pd30 nanowires from a complexed ammonium-sulfosalicylic electrolyte with high stability [J].
Haehnel, V. ;
Faehler, S. ;
Schultz, L. ;
Schloerb, H. .
ELECTROCHEMISTRY COMMUNICATIONS, 2010, 12 (08) :1116-1119
[18]   Fabrication, Microstructure, and Properties of Nanoporous Pd, Ni, and Their Alloys by Dealloying [J].
Hakamada, Masataka ;
Mabuchi, Mamoru .
CRITICAL REVIEWS IN SOLID STATE AND MATERIALS SCIENCES, 2013, 38 (04) :262-285
[19]   Preparation of Nanoporous Palladium by Dealloying: Anodic Polarization Behaviors of Pd-M (M = Fe, Co, Ni) Alloys [J].
Hakamada, Masataka ;
Mabuchi, Mamoru .
MATERIALS TRANSACTIONS, 2009, 50 (03) :431-435
[20]   Electrodeposition and characterization of Fe80Ga20 alloy films [J].
Iselt, D. ;
Gaitzsch, U. ;
Oswald, S. ;
Faehler, S. ;
Schultz, L. ;
Schloerb, H. .
ELECTROCHIMICA ACTA, 2011, 56 (14) :5178-5183