Simple Synthesis of micrometer Fe3O4 particles with controlled magnetic behaviors

被引:0
作者
Zhao, Guizhe [1 ]
Zhou, Xing [1 ]
Liu, Yaqing [1 ]
Sun, Youyi [1 ]
机构
[1] N Univ China, Res Ctr Engn Technol Polymer Composites Shanxi Pr, Taiyuan 030051, Peoples R China
来源
SOFT MAGNETIC MATERIALS | 2011年 / 298卷
关键词
Fe3O4; particles; magnetic properties; size control; polyethylene glycol; NANOPARTICLES; SIZE;
D O I
10.4028/www.scientific.net/AMR.298.273
中图分类号
TB33 [复合材料];
学科分类号
摘要
Fe3O4 particles were prepared by the co-precipitating method in the presence of polyethylene glycol (PEG). They were characterized by the Transmittance electron microscopy (TEM) and Fourier transform infrared (FT-IR) spectroscope, which indicate the formation of spherical Fe3O4 particles with a wide range of sizes (up to 200 nm in radius) and the polydispersity of particle size below 20%. Furthermore, the magnetic properties of Fe3O4 particles were measured using a vibrating sample magnetometer (VSM), indicating that the particles possess high saturation magnetization at room temperature. These results are attributed that the Fe3O4 particles were directly coated with PEG in a seeded growth Sto ber process.
引用
收藏
页码:273 / 277
页数:5
相关论文
共 10 条
[1]   Formation of a three-dimensional microstructure of Fe3O4-poly(vinyl alcohol) composite by evaporating the hydrosol under a magnetic field [J].
Abu-Much, R ;
Meridor, U ;
Frydman, A ;
Gedanken, A .
JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (16) :8194-8203
[2]   Synthesis of ultra-fine particles of strontium hexaferrite by a modified co-precipitation method [J].
Ataie, A ;
Heshmati-Manesh, S .
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2001, 21 (10-11) :1951-1955
[3]   Influence of metal content on size, dispersion, and magnetic properties of iron-cobalt alloy nanoparticles embedded in silica matrix [J].
Ennas, G ;
Falqui, A ;
Marras, S ;
Sangregorio, C ;
Marongiu, G .
CHEMISTRY OF MATERIALS, 2004, 16 (26) :5659-5663
[4]   Morphology control and texture of Fe3O4 nanoparticle-coated polystyrene microspheres by ethylene glycol in forced hydrolysis reaction [J].
Huang, ZB ;
Tang, FQ ;
Zhang, L .
THIN SOLID FILMS, 2005, 471 (1-2) :105-112
[5]   Synthesis of Fe3O4 nanoparticles with various sizes and magnetic properties 14 by controlled hydrolysis [J].
Iida, Hironori ;
Takayanagi, Kosuke ;
Nakanishi, Takuya ;
Osaka, Tetsuya .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 2007, 314 (01) :274-280
[6]   Magnetic nanoparticles:: Synthesis, protection, functionalization, and application [J].
Lu, An-Hui ;
Salabas, E. L. ;
Schueth, Ferdi .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2007, 46 (08) :1222-1244
[7]   Synthesis of magnetite (Fe3O4) nanoparticles without surfactants at room temperature [J].
Martinez-Mera, I. ;
Espinosa-Pesqueira, M. E. ;
Perez-Hernandez, R. ;
Arenas-Alatorre, J. .
MATERIALS LETTERS, 2007, 61 (23-24) :4447-4451
[8]   Formation, characterization, and magnetic properties of Fe3O4 nanowires encapsulated in carbon microtubes [J].
Xu, LQ ;
Zhang, WQ ;
Ding, YW ;
Peng, YY ;
Zhang, SY ;
Yu, WC ;
Qian, YT .
JOURNAL OF PHYSICAL CHEMISTRY B, 2004, 108 (30) :10859-10862
[9]   The colloidal stability and core-shell structure of magnetite nanoparticles coated with alginate [J].
Xu, X. Q. ;
Shen, H. ;
Xu, J. R. ;
Xie, M. Q. ;
Li, X. J. .
APPLIED SURFACE SCIENCE, 2006, 253 (04) :2158-2164
[10]   Solvothermal synthesis and characterization of size-controlled Fe3O4 nanoparticles [J].
Yan, Aiguo ;
Liu, Xiaohe ;
Qiu, Guanzhou ;
Wu, Hongyi ;
Yi, Ran ;
Zhang, Ning ;
Xu, Jing .
JOURNAL OF ALLOYS AND COMPOUNDS, 2008, 458 (1-2) :487-491