Visible-light-mediated facile synthesis of disulfides using reusable TiO2/MoS2 nanocomposite photocatalyst

被引：14

作者：

Liu, Wenjie ^{[1
]}

Wang, Cancan ^{[1
]}

Huang, Yibo ^{[1
,2
]}

Chen, Qun ^{[1
]}

Wang, Liang ^{[1
]}

He, Mingyang ^{[1
]}

机构：

[1] Changzhou Univ, Sch Petrochem Engn, Changzhou 213164, Peoples R China

[2] Changzhou Inst Engn & Technol, Dept Pharm, Changzhou, Peoples R China

来源：

SYNTHETIC COMMUNICATIONS | 2016年 / 46卷 / 15期

基金：

中国国家自然科学基金;

关键词：

Disulfides; photocatalysis; semiconductor; TiO2; MoS2; nanocomposite; EFFICIENT SYNTHESIS; AEROBIC OXIDATION; THIOLS; GRAPHENE; MOS2; SULFIDES;

D O I：

10.1080/00397911.2016.1199808

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A nontoxic and inexpensive TiO2/MoS2 nanocomposite was prepared and employed as an efficient photocatalyst for the synthesis of symmetrical disulfides under visible light irradiation at room temperature. Both aryl and alkyl thiols survived the reaction conditions, affording the corresponding disulfides in good to excellent yields. The photocatalyst could be easily recovered by simple centrifugation and filtration and reused several times without significant loss in its activity. [GRAPHICS]

引用

页码：1268 / 1274

页数：7

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