Chromatographic NMR

被引:10
作者
Caldarelli, Stefano [1 ]
机构
[1] Aix Marseille Univ, ISm2, UMR 6263, Marseille, France
来源
ANNUAL REPORTS ON NMR SPECTROSCOPY, VOL 73 | 2011年 / 73卷
关键词
Mixtures; Porous materials; Diffusion; HRMAS; DOSY; NUCLEAR-MAGNETIC-RESONANCE; ANGLE-SPINNING NMR; SELF-DIFFUSION MEASUREMENTS; HIGH-RESOLUTION; LIQUID-CHROMATOGRAPHY; PARMIGIANO-REGGIANO; SOLID-STATE; HR/MAS NMR; ECHO NMR; GRADIENT;
D O I
10.1016/B978-0-08-097074-5.00005-0
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
The principle of chromatographic NMR, a version of NMR diffusometry devised for a facilitated study of mixtures using the addition of a selectively retarding agent, is illustrated. The technical requirements for acquiring exploitable 1 H NMR diffusometry spectra for a heterogeneous solution/solid mix are described. Applications of the technique to test mixtures for several choices of solvents/ interacting phase are reviewed.
引用
收藏
页码:159 / 173
页数:15
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