Synchrotron X-ray diffraction experiments with a prototype hybrid pixel detector

被引:32
作者
Le Bourlot, C. [2 ,4 ]
Landois, P. [1 ]
Djaziri, S. [3 ]
Renault, P. -O. [3 ]
Le Bourhis, E. [3 ]
Goudeau, P. [3 ]
Pinault, M. [5 ]
Mayne-L'Hermite, M. [5 ]
Bacroix, B. [2 ]
Faurie, D. [2 ]
Castelnau, O. [4 ]
Launois, P. [1 ]
Rouziere, S. [1 ]
机构
[1] Univ Paris 11, LPS, CNRS, UMR8502, F-91405 Orsay, France
[2] Univ Paris 13, CNRS, LSPM, Inst Galilee, F-93430 Villetaneuse, France
[3] Univ Poitiers, Inst Pprime, CNRS, ENSMA,UPR 3346, F-86962 Futuroscope, France
[4] Arts & Metiers ParisTech, PIMM, CNRS, F-75013 Paris, France
[5] CEA Saclay, LFP, CEA, CNRS,URA 2453, F-91191 Gif Sur Yvette, France
关键词
synchrotron X-ray diffraction; pixel area detectors; calibration; ELASTIC-ANISOTROPY; THIN-FILMS; IN-SITU; GROWTH; PILATUS; CDTE;
D O I
10.1107/S0021889811049107
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A prototype X-ray pixel area detector (XPAD3.1) has been used for X-ray diffraction experiments with synchrotron radiation. The characteristics of this detector are very attractive in terms of fast readout time, high dynamic range and high signal-to-noise ratio. The prototype XPAD3.1 enabled various diffraction experiments to be performed at different energies, sample-to-detector distances and detector angles with respect to the direct beam, yet it was necessary to perform corrections on the diffraction images according to the type of experiment. This paper is focused on calibration and correction procedures to obtain high-quality scientific results specifically developed in the context of three different experiments, namely mechanical characterization of nanostructured multilayers, elasticplastic deformation of duplex steel and growth of carbon nanotubes.
引用
收藏
页码:38 / 47
页数:10
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