Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection

被引：4
|
作者：
Kuang, Wenjun [1 ,2 ,3 ]
Wu, Xinqiang [1 ]
Wang, Xiang [1 ]
Han, En-Hou [1 ]
机构：
[1] Chinese Acad Sci, Inst Met Res, Key Lab Nucl Mat & Safety Assessment, Liaoning Key Lab Safety & Assessment Tech Nucl Ma, Shenyang 110016, Peoples R China
[2] Univ Michigan, Ann Arbor, MI 48109 USA
[3] Chinese Acad Sci, Inst Met Res, Shenyang 110016, Peoples R China
来源：
CORROSION | 2015年 / 71卷 / 06期
关键词：
cracking; oxidation; Raman spectroscopy; HYDROTHERMAL CONDITIONS; STAINLESS-STEEL; OXIDE-FILM; ELEVATED-TEMPERATURES; OXYGEN CONCENTRATION; ALLOY; 690; WATER; CORROSION; IRON; 304-STAINLESS-STEEL;
D O I：
10.5006/1617
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A window was developed on a high-temperature, high-pressure refreshed autoclave to perform in situ tests. High-purity single crystal sapphire was used as window material to withstand the harsh environment and minimize the production of fluorescence. The cone-shaped internal structure enables a large light flux necessary for the in situ optical observation. Through this window, in situ optical observation and Raman tests were successfully performed in high-temperature, high-pressure water using a long-distance microscope and a custom-made Raman system. The formation of spinel oxide on 304 stainless steel in oxygenated water containing a high concentration of Ni cations was verified by in situ Raman tests.
引用
收藏
页码：687 / 691
页数：5
相关论文
共 50 条
  • [41] High-pressure high -temperature Raman spectroscopy of kerogen: Relevance to subducted organic carbon
    Childress, Laurel B.
    Jacobsen, Steven D.
    AMERICAN MINERALOGIST, 2017, 102 (1-2) : 391 - 403
  • [42] Technical note:: Detection of soluble species released during metal corrosion in high-temperature aqueous solutions
    Bojinov, M
    Kinnunen, P
    Laitinen, T
    Mäkelä, K
    Mäkelä, M
    Saario, T
    Sirkiä, P
    CORROSION, 2001, 57 (05) : 387 - 393
  • [43] In situ observation of crystallographic preferred orientation of deforming olivine at high pressure and high temperature
    Ohuchi, Tomohiro
    Nishihara, Yu
    Seto, Yusuke
    Kawazoe, Takaaki
    Nishi, Masayuki
    Maruyama, Genta
    Hashimoto, Mika
    Higo, Yuji
    Funakoshi, Ken-ichi
    Suzuki, Akio
    Kikegawa, Takumi
    Irifune, Tetsuo
    PHYSICS OF THE EARTH AND PLANETARY INTERIORS, 2015, 243 : 1 - 21
  • [44] High-pressure Raman study of Terephthalonitrile
    Li, DongFei
    Zhang, KeWei
    Song, MingXing
    Zhai, NaiCui
    Sun, ChengLin
    Li, HaiBo
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2017, 173 : 376 - 382
  • [45] In situ High-Temperature Experiments
    Neuville, Daniel R.
    Hennet, Louis
    Florian, Pierre
    de Ligny, Dominique
    SPECTROSCOPIC METHODS IN MINERALOLOGY AND MATERIALS SCIENCES, 2014, 78 : 779 - 800
  • [46] Effect of Ammonia on Methane Hydrate Stability under High-Pressure and High-Temperature Conditions
    Kadobayashi, Hirokazu
    Hirai, Hisako
    Ohfuji, Hiroaki
    Kawamura, Hideaki
    Muraoka, Michihiro
    Yoshida, Suguru
    Yamamoto, Yoshitaka
    JOURNAL OF PHYSICAL CHEMISTRY A, 2020, 124 (51): : 10890 - 10896
  • [47] Mechanisms and mechanical properties of high-temperature high-pressure sintered vanadium carbide ceramics
    Chen, Jie
    Peng, Fang
    Wang, Yipeng
    He, Ruiqi
    Zhang, Zhengang
    Liang, Wenjia
    Long, Haidong
    He, Peihong
    Liang, Hao
    INTERNATIONAL JOURNAL OF REFRACTORY METALS & HARD MATERIALS, 2024, 118
  • [48] HIGH-TEMPERATURE HIGH-PRESSURE EXPERIMENTS ON H2O-N2
    VANHINSBERG, MGE
    VERBRUGGE, R
    SCHOUTEN, JA
    FLUID PHASE EQUILIBRIA, 1993, 88 : 115 - 121
  • [49] Iodine-mediated high-pressure high-temperature carbonization of hydrocarbons and synthesis of nanodiamonds
    Ekimov, E. A.
    Kondrina, K. M.
    Zibrov, I. P.
    Lyapin, S. G.
    Lovygin, M., V
    Kazanskiy, P. R.
    MATERIALS RESEARCH BULLETIN, 2021, 137
  • [50] Effects of CH4 and CO2 on the sulfidization of goethite and magnetite: an in situ Raman spectroscopic study in high-pressure capillary optical cells at room temperature
    Wang, Menghan
    Chou, I-Ming
    Lu, Wanjun
    De Vivo, Benedetto
    EUROPEAN JOURNAL OF MINERALOGY, 2015, 27 (02) : 193 - 201
12345