Synthesis of α-Fe2O3 nanobelts and nanoflakes by thermal oxidation and study to their magnetic properties

被引：30
|
作者：
Su, Xinghua [2 ]
Yu, Chengshou [1 ]
Qiang, Chengwen [1 ,3 ]
机构：
[1] Lanzhou Univ, Dept Mat Sci & Engn, Lanzhou 730000, Peoples R China
[2] Changan Univ, Sch Mat Sci & Engn, Xian 710061, Peoples R China
[3] Chinese Acad Sci, China & Inst Modern Phys, Lanzhou 730000, Peoples R China
来源：
APPLIED SURFACE SCIENCE | 2011年 / 257卷 / 21期
关键词：
Hematite; Nanobelts; Nanoflakes; Magnetic property; LITHIUM-ION BATTERY; NANOTUBES; NANORODS; GROWTH; NANOPARTICLES; FE2O3; UNIFORM; ARRAYS; SENSOR; AREA;
D O I：
10.1016/j.apsusc.2011.05.091
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
alpha-Fe2O3 nanobelts and nanoflakes have been successfully synthesized by oxidation of iron-coated ITO glass in air. The X-ray diffraction, Raman spectrum and scanning electron microscopy are carried out to characterize the nanobelts and nanoflakes. The formation mechanism has been presented. Significantly, the magnetic investigations show that the magnetic properties are strongly shape-dependent. The magnetization measurements of belt-like and flake-like alpha-Fe2O3 in perpendicular exhibit ferromagnetic feature with the coercivity (H-c) and saturation magnetization (M-s) of 334.5 Oe and 1.35 emu/g, 239.5 Oe and 0.12 emu/g, respectively. For the parallel, belt-like and flake-like alpha-Fe2O3 also exhibit ferromagnetic feature with the Hc and Ms of 205.5 Oe and 1.44 emu/g, 159.6 Oe and 0.15 emu/g, respectively. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码：9014 / 9018
页数：5
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