Synthesis, Characterization and Hirshfeld Surface Analysis of a 2-thiophene Acetic Acid Derivative

被引：3

作者：

Rani, N. Latha ^{[1
]}

Chakravarthy, M. P. ^{[2
]}

Mohana, K. N. ^{[2
]}

Lokanath, N. K. ^{[1
]}

Sridhar, M. A. ^{[1
]}

机构：

[1] Univ Mysore, Dept Studies Phys, Mysore 570006, Karnataka, India

[2] Univ Mysore, Dept Studies Chem, Mysore 570006, Karnataka, India

来源：

MOLECULAR CRYSTALS AND LIQUID CRYSTALS | 2015年 / 607卷 / 01期

关键词：

fingerprint plots; 2-thiophene acetic acid; Candida albicans; Hirshfeld surface analysis; FTIR spectrum; INTERMOLECULAR INTERACTIONS;

D O I：

10.1080/15421406.2014.928978

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

N,N '-dicyclohexylcarbamoyl-2-(thiophen-2-yl)acetamide (C19H28N2 O2S), was prepared using 1,3-dicyclohexylurea. The compound has been characterized by IR, and single-crystal X-ray diffraction followed by a detailed Hirshfeld surface analysis. The compound crystallizes in the monoclinic space group P2(1)/c, with cell parameters a = 9.0969(3) angstrom, b = 18.3067(5) angstrom, c = 11.6499(3) angstrom, beta = 103.876(2)degrees, V = 1883.49(10) angstrom(3), Z = 4. The crystal structure of the compound is stabilized by the intermolecular interactions of types N-H horizontal ellipsis O, C-H horizontal ellipsis O and intramolecular interactions of the type C-H horizontal ellipsis O.

引用

页码：223 / 231

页数：9