Complexity of the relationships between the sintering-temperature-dependent grain size, airborne-particle abrasion, ageing and strength of 3Y-TZP ceramics

被引:35
作者
Cotic, Jasna [1 ]
Jevnikar, Peter [1 ]
Kocjan, Andraz [2 ]
Kosmac, Tomaz [2 ]
机构
[1] Univ Ljubljana, Fac Med, Dept Prosthodont, Hrvatski Trg 6, SI-1000 Ljubljana, Slovenia
[2] Jozef Stefan Inst, Dept Ceram Engn, Jamova 39, SI-1000 Ljubljana, Slovenia
关键词
Zirconia; Sintering temperature; Grain size; Airborne-particle abrasion; Low-temperature degradation; PHASE-TRANSFORMATION; FLEXURAL STRENGTH; HYDROTHERMAL DEGRADATION; ZIRCONIA; SURFACE; RELIABILITY; FUTURE;
D O I
10.1016/j.dental.2015.12.004
中图分类号
R78 [口腔科学];
学科分类号
1003 ;
摘要
Objectives. This study was designed to explore the complex relationships between the sintering-temperature-dependent grain size, airborne-particle abrasion, ageing and strength of 3Y-TZP ceramics. Methods. Biomedical grade 3Y-TZP powder was used to fabricate 180 discs. Half of them were sintered at 1400 degrees C for 2 h and half at 1500 degrees C for 2 h. A total of 18 groups of 10 were formed and subjected to the fully crossed experimental protocol of airborne-particle abrasion with Al2O3 at 2.5 bar (no abrasion, 50 mu m, 110 mu m) and accelerated ageing at 134 degrees C (no ageing, 12 h, 48 h). The relative amount of monoclinic phase was determined with XRD. The biaxial flexural strength was measured and statistically analyzed using the three-way ANOVA followed by predetermined contrasts and Tukey's HSD test (alpha = 0.05). Results. The low-temperature-sintered, fine-grained ceramic exhibited an excellent ageing resistance, while the high-temperature-sintered, coarse-grained ceramic experienced a higher surface strengthening and a substantially improved ageing resistance with respect to the airborne-particle abrasion. The overall performance of this material was superior. Significance. Our results show that the sintering temperature has a minor effect on the flexural strength, but it plays a crucial role in the surface strengthening and the ageing behaviour of 3Y-TZP dental ceramics. (C) 2015 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码:510 / 518
页数:9
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