Synthesis and crystal structure of Ni(II) complexes of 2′-(3,5-dibromo-2-hydroxybenzylidene)-3,5-dihydroxybenzoylhydrazide

被引：2
|
作者：
Yang, Jian-Guo [1 ]
Pan, Fu-You [1 ]
Jia, Wen-Ping [1 ]
Li, Fang [1 ]
机构：
[1] Taizhou Univ, Dept Chem, Taizhou 317000, Zhejiang, Peoples R China
来源：
JOURNAL OF COORDINATION CHEMISTRY | 2008年 / 61卷 / 11期
关键词：
nickel(II); 3,5-dihydroxybenzoylhydrazide; crystal structure; synthesis;
D O I：
10.1080/00958970701746659
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A new mononuclear nickel(II) complex incorporating a Schiff-base ligand, [NiL2](DMF)(4) (HL = 2'-(3,5-dibromo-2-hydroxybenzylidene)-3,5-dihydroxybenzoylhydrazide), has been synthesized and characterized by IR, UV-Vis, elemental analysis and X-ray crystal structure analysis. HL is an anionic tridentate ligand. The nickel atom is hexacoordinated with two oxygen atoms from keto group and two oxygen atoms from hydroxy group and two nitrogen atoms from amide, with the two nitrogen atoms occupying the axial positions forming a distorted octahedral coordination sphere.
引用
收藏
页码：1759 / 1764
页数：6
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