3-{2-[(3-{(E)-2-[4-(Dimethylamino)phenyl]ethenyl}quinoxalin-2-yl)oxy]ethyl}-1,3-oxazolidin-2-one monohydrate

被引：2

作者：

Ramli, Youssef ^{[4
]}

Zouihri, Hafid ^{[3
]}

Essassi, El Mokhtar ^{[4
]}

Ng, Seik Weng ^{[1
,2
]}

机构：

[1] Univ Malaya, Dept Chem, Kuala Lumpur 50603, Malaysia

[2] King Abdulaziz Univ, Dept Chem, Jeddah 21413, Saudi Arabia

[3] Angle Allal Fassi FAR, CNRST Div UATRS, Rabat, Morocco

[4] Univ Mohammed V Agdal, Lab Chim Organ Heterocycl, Rabat, Morocco

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2012年 / 68卷

关键词：

Data-to-parameter ratio = 20.1; Mean σ(C-C) = 0.002 Å; R factor = 0.046; Single-crystal X-ray study; T = 293 K; wR factor = 0.137;

D O I：

10.1107/S1600536811054481

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C(23)H(24)N(4)O(3)center dot H(2)O, the 1,3-oxazoline ring is nearly planar [maximum deviation = 0.059 (2) angstrom] and its mean plane is twisted by 30.12 (8)degrees with respect to the quinoxaline fused-ring system; the benzene ring is nearly coplanar with the quinoxaline fused-ring system [dihedral angle = 2.52 (2)degrees]. The water molecule of crystallization is hydrogen-bond donor to an N atom of the quinoxaline ring system as well as an O atom of the oxazolinone unit, the two hydrogen bonds generating a chain running along the c axis.

引用

页数：10

共 50 条

[31] (2E)-1-(2,4-Dichlorophenyl)-3-[3-(4-nitrophenyl)-1-phenyl-1-H-pyrazol-4-yl]-prop-2-en-1-one
Isloor, Arun M.
Malladi, Shridhar
Gerber, Thomas
van Brecht, Benjamin
Betz, Richard
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O616 - U1505
[32] 2-[3-(1,3-Benzothiazol-2-yl)-2,2-dimethylpropyl]-2-methyl-2,3-dihydro-1,3-benzothiazole
Yousuf, Sammer
Siddiqui, Hina
Farooq, Rabia
Choudhary, M. Iqbal
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02349 - +
[33] (E)-3-[(Dimethylamino)methylidene]-4-phenyl-1H-1,5-benzodiazepin-2(3H)-one
Loughzail, Mohamed
Baouid, Abdesselam
Fernandes, Jose A.
Driss, Mohamed
Soumhi, El Hassane
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 0126 - +
[34] (2E)-3-[4-(Benzyloxy)phenyl]-1-(2,6-dichloro-3-fluorophenyl)prop-2-en-1-one
Praveen, Aletti S.
Yathirajan, Hemmige S.
Gerber, Thomas
van Brecht, Benjamin
Betz, Richard
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O3386 - +
[35] 6-Bromo-1-[2-(2-oxo-1,3-oxazolidin-3-yl)ethyl]-1H-imidazo[4,5-b]pyridin-2(3H)-one
Bel-Ghacham, H.
Rodi, Y. Kandri
Saffon, Natalie
Essassi, El Mokhtar
Ng, Seik Weng
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O456 - U3350
[36] Ethyl 3-(4-methoxyphenyl)-2-phenyl-3-(4-phenyl-1,2,3-selenadiazol-5-yl)-propanoate
Sugumar, P.
Sankari, S.
Manisankar, P.
Ponnuswamy, M. N.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02347 - +
[37] Ethyl 2-(4-nitrophenyl)-1-[3-(2-oxopyrrolidin-1-yl)propyl]-1H-benzimidazole-5-carboxylate
Yoon, Yeong Keng
Ali, Mohamed Ashraf
Choon, Tan Soo
Asik, Safra Izuani Jama
Razak, Ibrahim Abdul
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : O59 - +
[38] Ethyl 3-(4-chlorophenyl)-2-phenyl-3-(4phenyl-1,2,3-selenadiazol-5-yl) propanoate
Sugumar, P.
Sankari, S.
Manisankar, P.
Thiruselvam, V.
Ponnuswamy, M. N.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1239 - +
[39] 3-(2-Methylamino-1,3-thiazol-4-yl)-2H-chromen-2-one
Yusufzai, Samina Khan
Osman, Hasnah
Rahim, Aisyah Saad Abdul
Arshad, Suhana
Razak, Ibrahim Abdul
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02416 - +
[40] (E)-3-(4-Methylphenyl)-1-(1,3-thiazol-2-yl)prop-2-en-1-one
Palaniappan, Annamalai
Arulmozhivarman, Arumugam
Ramachandran, Rajamanickam
Srinivasan, Subramanian
Senthan, Sivakolunthu
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1875 - +

← 1 2 3 4 5 →