Synthesis of vicinal bis(alkylthio) derivatives by reductive coupling of dithioacetals derived from aromatic aldehydes with low valent titanium iodide species

被引：0
|
作者：
Yoshimura, N [1 ]
Igarashi, K [1 ]
Funasaka, S [1 ]
Mukaiyama, T [1 ]
机构：
[1] Sci Univ Tokyo, Fac Sci, Dept Appl Chem, Shinjuku Ku, Tokyo 1628601, Japan
来源：
CHEMISTRY LETTERS | 2001年 / 07期
关键词：
D O I：
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中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Reduction of dithioacetals derived from aromatic aldehydes with low valent titanium iodide species in situ formed by treatment of titanium(IV) iodide with zinc in a mixed solvent of dichloromethane and pivalonitrile at room temperature afforded coupling products, vicinal bis(alkylthio) derivatives, in good to high yields.
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页码：640 / 641
页数：2
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