Redetermination of Te6[AsF6]4•2SO2 at 125 K

被引：8
作者：
Beck, J [1 ]
Steden, F [1 ]
机构：
[1] Univ Bonn, Inst Anorgan Chem, D-53121 Bonn, Germany
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2003年 / 59卷
关键词：
D O I：
10.1107/S1600536803024887
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The crystal structure of the title compound, hexatellurium tetrakis(hexafluoroarsenate) sulfur dioxide disolvate, Te-6[AsF6](4).2SO(2), was first determined by Burns, Gillespie, Luk & Slim [Inorg. Chem. (1979), 18, 3086-3094]. We present here a redetermination at low temperature and of improved precision, in which all atoms were refined with anisotropic displacement parameters.
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页码：I158 / I160
页数：3
相关论文
共 14 条
  • [1] [Anonymous], COLLECT
  • [2] [Anonymous], 1993, HABITUS
  • [3] Synthesis, crystal structure, and solid state phase transition of Te4[AsF6]2•SO2
    Beck, J
    Steden, F
    Reich, A
    Fölsing, H
    [J]. ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2003, 629 (06): : 1073 - 1079
  • [4] BERNDT M, 2001, DIAMOND VERSION 2 1E
  • [5] Recent advances in the understanding of the syntheses, structures, bonding and energetics of the homopolyatomic cations of Groups 16 and 17
    Brownridge, S
    Krossing, I
    Passmore, J
    Jenkins, HDB
    Roobottom, HK
    [J]. COORDINATION CHEMISTRY REVIEWS, 2000, 197 : 397 - 481
  • [6] PREPARATION, SPECTROSCOPIC PROPERTIES, AND CRYSTAL-STRUCTURES OF TE6(ASF6)4.2ASF3 AND TE6(ASF6)4.2SO2 - NEW TRIGONAL-PRISMATIC CLUSTER CATION, TE-6(4+)
    BURNS, RC
    GILLESPIE, RJ
    LUK, WC
    SLIM, DR
    [J]. INORGANIC CHEMISTRY, 1979, 18 (11) : 3086 - 3094
  • [7] CARDINAL G, 1982, INORG CHEM, V21, P765
  • [8] COLLINS HJ, 1987, INORG CHEM, V26, P1467
  • [9] The poly(heptatellurium) dication: A new twist
    Drake, GW
    Schimek, GL
    Kolis, JW
    [J]. INORGANIC CHEMISTRY, 1996, 35 (06) : 1740 - &
  • [10] CRYSTAL HANDLING AT LOW-TEMPERATURES
    KOTTKE, T
    STALKE, D
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1993, 26 : 615 - 619
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