Oxidation-resistant ZrB2-SiC composites at 2200 °C

被引:303
作者
Han, Jiecai [1 ]
Hu, Ping [1 ]
Zhang, Xinghong [1 ]
Meng, Songhe [1 ]
Han, Wenbo [1 ]
机构
[1] Harbin Inst Technol, Ctr Composite Mat, Harbin 150001, Peoples R China
基金
中国国家自然科学基金; 高等学校博士学科点专项科研基金;
关键词
ultra-high-temperature ceramic (UHTC); ZrB2; SiC; oxidation resistance;
D O I
10.1016/j.compscitech.2007.08.017
中图分类号
TB33 [复合材料];
学科分类号
摘要
Oxidation resistance tests were carried out on hot-pressed Zi-B-2-20 vol%SiC using an oxyacetylene torch. The temperature of the oxidized specimens exceeded 2200 degrees C. The mass and linear oxidation rates of the ZrB2-20 vol%SiC composites for 10 min were -0.23 mg/s and 0.66 mu m/s, respectively. The surface layer appeared dense and adherent with the exception of a few burst bubbles and craterlets. No macro-cracks or spallation were detected after oxidation, suggesting that these composites possess a super oxidation resistance. The microstructure of the surface and cross-section of the oxidized specimens were studied by scanning electron microscopy along with energy dispersive spectrometry and X-ray diffraction. The oxidation mechanism was also discussed. (c) 2007 Elsevier Ltd. All rights reserved.
引用
收藏
页码:799 / 806
页数:8
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