Crystal structure of N,N′-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropane

被引:2
作者
Khalaji, A. D. [1 ]
Fejfarova, K. [2 ]
Dusek, M. [2 ]
机构
[1] Golestan Univ, Fac Sci, Dept Chem, Gorgan, Iran
[2] ASCR, Inst Phys, Prague 18221 8, Czech Republic
关键词
X-ray diffraction; orthorhombic symmetry; Schiff base; SCHIFF-BASE;
D O I
10.1134/S0022476611060175
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The Schiff-base compound N,N'-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropan, (2,5-MeO-ba)(2)pn, is synthesized and characterized by elemental analysis, FT-IR and H-1 NMR spectroscopy. The crystal structure of (2,5-MeO-ba)(2)pn is determined by X-ray single crystal diffraction analysis. The X-ray diffraction analysis at 120 K reveals that (2,5-MeO-ba)(2)pn crystallizes in the orthorhombic system, Fdd2 space group with a = 29.339(9) , b = 29.4073(11) , c = 4.4524(2) , V = 3840.8(3) (3), mu = 0.72 mm(-1), and Z = 8.
引用
收藏
页码:1131 / 1133
页数:3
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