The distribution and evolution of ferroelectric and ferroelastic nanodomains in a polycrystalline (001)-oriented thin film of the simple multiferroic PbZr0.3Ti0.7O3 (PZT) are presented. With an external electric field applied between the probe tip and the PZT sample, ferroelastic domains were switched by rotating both in and out of plane, with partial conversion from a-oriented regions to c-oriented regions. After multiple such cycles, grains were observed to buckle as a direct consequence of the lateral size change arising from the conversion towards complete c-orientation. The factors determining the measured deflection of the cantilever in piezoresponse force microscopy were explored, highlighting the conditions under which quantitative or qualitative information may be obtained.
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No Illinois Univ, Dept Phys, De Kalb, IL 60115 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
Thompson, Carol
Fong, D. D.
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Argonne Natl Lab, Div Mat Sci, Argonne, IL 60439 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
Fong, D. D.
Wang, R. V.
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Argonne Natl Lab, Div Mat Sci, Argonne, IL 60439 USA
Argonne Natl Lab, Ctr Nanoscale Mat, Argonne, IL 60439 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
Wang, R. V.
Jiang, F.
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Argonne Natl Lab, Div Mat Sci, Argonne, IL 60439 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
Jiang, F.
Streiffer, S. K.
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Argonne Natl Lab, Ctr Nanoscale Mat, Argonne, IL 60439 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
Streiffer, S. K.
Latifi, K.
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No Illinois Univ, Dept Phys, De Kalb, IL 60115 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
Latifi, K.
Eastman, J. A.
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Argonne Natl Lab, Div Mat Sci, Argonne, IL 60439 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
Eastman, J. A.
Fuoss, P. H.
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Argonne Natl Lab, Div Mat Sci, Argonne, IL 60439 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
Fuoss, P. H.
Stephenson, G. B.
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Argonne Natl Lab, Div Mat Sci, Argonne, IL 60439 USA
Argonne Natl Lab, Ctr Nanoscale Mat, Argonne, IL 60439 USANo Illinois Univ, Dept Phys, De Kalb, IL 60115 USA
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Penn State Univ, Dept Mat Sci & Engn, University Pk, PA 16802 USA
Rice Univ, Dept Mat Sci & Nanoengn, Houston, TX 77005 USAUniv Sydney, Sch Aerosp Mech & Mechatron Engn, Sydney, NSW 2006, Australia
Hong, Liang
Wang, Feifei
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Shanghai Normal Univ, Dept Phys, Key Lab Optoelect Mat & Device, Shanghai 200234, Peoples R ChinaUniv Sydney, Sch Aerosp Mech & Mechatron Engn, Sydney, NSW 2006, Australia