3,3′-Bis(4-nitrophenyl)-1,1′-(p-phenylene)dithiourea dimethyl sulfoxide disolvate

被引:8
|
作者
Dong, Wen-Kui [1 ]
Yan, Hai-Bo [1 ]
Chai, Lan-Qin [1 ]
Lv, Zhong-Wu [1 ]
Zhao, Chun-Yu [1 ]
机构
[1] Lanzhou Jiaotong Univ, Sch Chem & Biol Engn, Lanzhou 730070, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷
关键词
D O I
10.1107/S160053680801430X
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The asymmetric unit of the title compound, C22H16N6O6S2 -2C(2)H(6)OS, consists of one half-molecule of the centrosymmetric thiourea derivative and one molecule of dimethyl sulfoxide ( DMSO). The carbonyl group forms an intramolecular hydrogen bond with the NH group, creating a six-membered (C-N-C-N-H center dot center dot center dot O) ring. Two other N - H center dot center dot center dot O hydrogen bonds link one molecule of the thiourea to two molecules of DMSO.
引用
收藏
页码:O1097 / U2353
页数:9
相关论文
共 50 条
  • [31] 3,3′-Dimethyl-1,1′-ethylenediimidazolium dibromide
    Chen, Yu
    Song, Wei
    Xu, Juan
    Cui, Rui-bo
    Tian, Dan-bi
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2454 - +
  • [32] FARBREAKTION DES 1-(4-NITROPHENYL)-3,3-DIALKYLTRIAZENS MIT ALKALHYDROXIDEN
    MATRAKA, M
    MARHOLD, J
    COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS, 1966, 31 (10) : 4178 - &
  • [33] 3,3′-Dibenzoyl-1,1′-(3,6-dioxaoctane-1,8-diyl)dithiourea
    Sow, Mouhamadou Moustapha
    Diouf, Ousmane
    Barry, Aliou Hamady
    Gaye, Mohamed
    Sall, Abdou Salam
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O569 - U2214
  • [34] 3,3′-[(4-Nitrophenyl)methylene]bis(4-hydroxy-2H-chromen-2-one)
    Ravikumar, N.
    Gopikrishna, G.
    Solomon, Anand
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : O265 - U1511
  • [35] 3,3′-(p-Phenylene)bis(3,4-dihydro-2H-1,3-benzoxazine)
    Ranjith, Sekaran
    Thenmozhi, Sundar
    Manikannan, Ramaiyan
    Muthusubramanian, Shanmugam
    Subbiahpandi, Arunachalathevar
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O581 - U2333
  • [36] 1,1′-bis(2-nitrophenyl)-5,5′-dipropyl-3,3′-bipyrazole
    Bouabdallah, I
    Ramdani, A
    Zidane, I
    Eddike, D
    Tillard, M
    Belin, C
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O4243 - O4245
  • [37] Accurate redeterminations of 1,1′-dibenzoylferrocene and (4-nitrophenyl)-ferrocene
    Gallagher, JF
    Ferguson, G
    Ahmed, SZ
    Glidewell, C
    Lewis, A
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1997, 53 : 1772 - 1775
  • [38] 1-(4-Nitrophenyl)-3-pivaloylthiourea
    Sultana, Sarwat
    Rauf, M. Khawar
    Ebihara, Masahiro
    Badshah, Amin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O2801 - U1880
  • [39] 3,3 '-Bis(chloromethyl)-4,4 '-diethoxy-1,1 '-biphenyl
    Trad, Hager
    Belkhiria, Mohamed Salah
    Majdoub, Mustapha
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O387 - +
  • [40] Reaction of 3,3′-bis(2-phenyl-5,5-dimethyl-4-oxopyrrolinylidene) 1,1′-dioxide with the methoxide anion
    Khalfina, Irina A.
    Vasilieva, Nadezhda V.
    Irtegova, Irina G.
    Reznikov, Vladimir A.
    Shundrin, Leonid A.
    MENDELEEV COMMUNICATIONS, 2012, 22 (06) : 327 - 329