Microstructure and Tensile Properties of SiC Reinforced Aluminum Matrix Composite Prepared by Selective Laser Melting

被引:12
作者
Zou Tianchun [1 ]
Zhu He [1 ]
Chen Minying [1 ]
Mei Siyuan [1 ]
Yang Xudong [2 ]
机构
[1] Civil Aviat Univ China, Coll Airworthiness, Tianjin 300300, Peoples R China
[2] Civil Aviat Univ China, Sino European Inst Aviat Engn, Tianjin 300300, Peoples R China
来源
CHINESE JOURNAL OF LASERS-ZHONGGUO JIGUANG | 2021年 / 48卷 / 10期
基金
俄罗斯科学基金会;
关键词
laser technique; laser materials processing; selective laser melting; aluminum matrix composite; microstructure; tensile properties; DENSIFICATION; BEHAVIOR;
D O I
10.3788/CJL202148.1002123
中图分类号
O43 [光学];
学科分类号
070207 ; 0803 ;
摘要
Objective Selective laser melting ( SLM) is an important method to realize functional optimization design and manufacture lightweight metal parts. The parts fabricated by SLM possess have a fine microstructure and excellent mechanical properties due to the rapid cooling rate. Some typical metals, such as aluminum alloys, Ni alloys, and Ti alloys, have been manufactured successfully by SLM and are used widely in the aerospace, automobile, and marine industries. In recent years, aluminum matrix composites have attracted considerable attention because of the advantageous properties of the matrix and reinforcement materials. Compared to other reinforced particles, SiC particles are the most common ceramic reinforcement because of their easy availability, low cost, and high hardness. However, few studies have examined the relative density, microstructure, and properties of SLMed SiC/Al composites, particularly the tensile properties. In this study, 5% SiC/AlSi7Mg composite specimens were prepared by SLM at different process parameters, and an almost entirely dense specimen was obtained. SiC particles and SiC, phases formed during the in situ reaction were distributed uniformly throughout the aluminum matrix, and strong metallurgical bond existed at the interface. Such aluminum matrix composites posse high tensile strength and yield strength but low ductility compared with the SLMed aluminum alloy. The fracture mode of the SLMed composites was mainly brittle fracture. Methods The original powders used in this study were SiC powders and gas atomized AISi7Mg powders. The mixed powders with 5% SiC powders were prepared using a V-type mixer. The SiC/AlSi7Mg composite specimens were then fabricated with SLM 125 equipment using different SLM process parameters in an argon atmosphere. Subsequently, the Archimedes method was used to measure the relative densities of the composite specimens. The microstructure of the SLMed composites was observed by optical microscopy and scanning electron microscopy after grinding, polishing, and etching in Keller reagent. The phase identification of the specimen was analyzed by X-ray diffraction. The tensile properties were examined using an electronic universal testing machine at room temperature. In addition, the fracture morphology of the composite was also characterized by scanning electron microscopy. Results and Discussions With increasing scanning speed and hatch spacing, the relative densities of the SLMed SiC/AlSi7Mg composites increased initially and then decreased ( Fig. 4). The relative density of the composite reached up to 99.2 % under the optimized process parameters ( laser power of 300 W, scanning speed of 1400 mm/s, hatch spacing of 0.12 mm, and layer thickness of 30 mu m). The typical fine zone, coarse zone, and heat-affected zone also can be found in the microstructure of the SLMed composite. New needle -like AI,SiC, phases formed during the SLM process because of the in situ reaction of SiC particles and molten aluminum matrix. The SiC particles and AI,SiC, phases were distributed uniformly in the matrix due to the Marangoni flow. The in situ reactions occurring on the surface of SiC particles promoted the wettability of the SiC particles and molten aluminum matrix. No pores or cracks were observed in the interface, indicating a strong metallurgical bonding. The SiC and AI,SiC, reinforced phases in the matrix enhanced matrix strength that could bear the stresses transferred from the matrix. However, they also hindered the dislocation movement and interface migration, and the deformation resistance of the composite was improved. The tensile strength and yield strength of the SLMed composite increased to 452 MPa and 280 MPa, respectively, but the elongation decreased to 4.5%. The cleavage plane observed in the fracture morphology also showed brittle fracture. Conclusions The SiC/AlSi7Mg composite specimens were manufactured successfully by the SLM process. The relative density of the SLMed composite increased initially and then decreased with increasing scanning speed and hatch spacing. The SLMed composite exhibited a relative density of 99. 2% under the optimized parameters. The microstructure of the composite was similar to the SLMed aluminum alloy, where the typical fine zone, coarse zone, and heat-affected zone exist. The new AI,SiC4-reinforced phases were formed in the aluminum matrix and at the interface of the SiC particles and matrix caused by the in situ reactions between the SiC particles and molten aluminum alloy. Good metallurgical bonding in the interface was formed. The SiC and AI,SiC,-reinforced phases were distributed uniformly throughout the aluminum matrix. The strength of the SLMed composite was improved by the addition of SiC particles and the formation of an Al4SiC, phase, but the ductility decreased compared to SLMed AlSi7Mg. The tensile strength, yield strength, and elongation of the SLMed composite were 452 MPa, 280 MPa, and 4. 5%, respectively. The fracture mode of the SLMed composites was mainly brittle fracture.
引用
收藏
页数:9
相关论文
共 22 条
[1]   Thermal behavior of the molten pool, microstructural evolution, and tribological performance during selective laser melting of TiC/316L stainless steel nanocomposites: Experimental and simulation methods [J].
AlMangour, Bandar ;
Grzesiak, Dariusz ;
Cheng, Jinquan ;
Ertas, Yavuz .
JOURNAL OF MATERIALS PROCESSING TECHNOLOGY, 2018, 257 :288-301
[2]   Microstructure and wear studies of laser clad Al-Si/SiC(p) composite coatings [J].
Anandkumar, R. ;
Almeida, A. ;
Colaco, R. ;
Vilar, R. ;
Ocelik, V. ;
De Hosson, J. Th. M. .
SURFACE & COATINGS TECHNOLOGY, 2007, 201 (24) :9497-9505
[3]   Selective laser melting of AlSi10 Mg: Influence of process parameters on Mg2Si precipitation and Si spheroidization [J].
Biffi, C. A. ;
Fiocchi, J. ;
Tuissi, A. .
JOURNAL OF ALLOYS AND COMPOUNDS, 2018, 755 :100-107
[4]   Selective laser melting of in-situ Al4SiC4+SiC hybrid reinforced Al matrix composites: Influence of starting SiC particle size [J].
Chang, Fei ;
Gu, Dongdong ;
Dai, Donghua ;
Yuan, Pengpeng .
SURFACE & COATINGS TECHNOLOGY, 2015, 272 :15-24
[5]   Experimental Research on Selective Laser Melting AlSi10Mg Alloys: Process, Densification and Performance [J].
Chen, Zhen ;
Wei, Zhengying ;
Wei, Pei ;
Chen, Shenggui ;
Lu, Bingheng ;
Du, Jun ;
Li, Junfeng ;
Zhang, Shuzhe .
JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE, 2017, 26 (12) :5897-5905
[6]   Recent developments in advanced aircraft aluminium alloys [J].
Dursun, Tolga ;
Soutis, Costas .
MATERIALS & DESIGN, 2014, 56 :862-871
[7]   Simultaneous enhancement of strength, ductility, and hardness of TiN/AlSi10Mg nanocomposites via selective laser melting [J].
Gao, C. ;
Wu, W. ;
Shi, J. ;
Xiao, Z. ;
Akbarzadeh, A. H. .
ADDITIVE MANUFACTURING, 2020, 34
[8]  
Gao W Y, 2020, HOT WORKING TECHNOLO, V49, P17
[9]   Laser Additive Manufacturing of High-Performance Metallic Aerospace Components [J].
Gu Dongdong ;
Zhang Hongmei ;
Chen Hongyu ;
Zhang Han ;
Xi Lixia .
CHINESE JOURNAL OF LASERS-ZHONGGUO JIGUANG, 2020, 47 (05)
[10]   Microstructures and mechanical properties of A356 (AlSi7Mg0.3) aluminum alloy fabricated by selective laser melting [J].
Kimura, Takahiro ;
Nakamoto, Takayuki .
MATERIALS & DESIGN, 2016, 89 :1294-1301