Synthesis, characterization and thermal behaviour of solid-state compounds of europium(III) and gadolinium(III) 3-methoxybenzoate

被引：1
|
作者：
Dametto, Patricia R. [1 ]
Ambrozini, Beatriz [1 ]
Siqueira, Adriano B. [1 ]
Carvalho, Claudio T. [1 ]
Ionashiro, Massao [1 ]
机构：
[1] Univ Estadual Paulista, Inst Quim, Araraquara, SP, Brazil
来源：
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY | 2009年 / 97卷 / 02期
基金：
巴西圣保罗研究基金会;
关键词：
Eu(III); Gd(III); 3-Methoxybenzoate; Thermal behaviour; AROMATIC SYSTEM; BENZOIC-ACID; LANTHANIDES; COMPLEXES;
D O I：
10.1007/s10973-009-0281-3
中图分类号：
O414.1 [热力学];
学科分类号：
摘要：
Solid-state Ln-C(8)H(7)O(3) compounds, where Ln stands for Eu(III) and Gd(III) and C(8)H(7)O(3) is 3-methoxybenzoate, have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, elemental analysis and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal stability and decomposition of the isolated compounds.
引用
收藏
页码：765 / 768
页数：4
相关论文
共 50 条
  • [41] Facile green synthesis of iron oxide nanoparticles via solid-state thermolysis of a chiral, 3D anhydrous potassium tris(oxalato)ferrate(III) precursor
    Saritha, A.
    Raju, B.
    Rao, D. Narayana
    Roychowdhury, A.
    Das, D.
    Hussain, K. A.
    ADVANCED POWDER TECHNOLOGY, 2015, 26 (02) : 349 - 354
  • [42] Coordination-Induced Formation of One-Dimensional Nanostructures of Europium Benzene-1,3,5-tricarboxylate and Its Solid-State Thermal Transformation
    Liu, Kai
    You, Hongpeng
    Jia, Guang
    Zheng, Yuhua
    Song, Yanhua
    Yang, Mei
    Huang, Yeju
    Zhang, Hongjie
    CRYSTAL GROWTH & DESIGN, 2009, 9 (08) : 3519 - 3524
  • [43] Synthesis, characterization and thermal behavior of solid state compounds of 2-chlorobenzylidenepyruvat with trivalent aluminium, gallium, indium and scandium metals
    Bannach, G
    Schnitzler, E
    Ionashiro, M
    ECLETICA QUIMICA, 2003, 28 (01): : 19 - 24
  • [44] Multi-stimuli fluorescent behaviour of boron compounds derived from hydrazones in the solid state (thermochromism, vapochromism, and piezochromism): Synthesis, characterization, and photophysical studies
    Ibarra-Rodriguez, Marisol
    Munoz-Flores, Blanca M.
    Jimenez-Perez, Victor M.
    JOURNAL OF LUMINESCENCE, 2018, 198 : 342 - 349
  • [45] Synthesis, solution and solid-state structure of Pd(II), Pt(II), Ir(III) and Zn(II) complexes with 5-pyridyl substituted N-methyl isoxazolidines
    Lysenko, AB
    Shishkina, SV
    Shishkin, OV
    Peralta-Pérez, E
    López-Ortiz, F
    Lampeka, RD
    POLYHEDRON, 2001, 20 (9-10) : 957 - 967
  • [46] Novel solid-state compounds of heavy rare-earth (III) picolinates. A pyrolytic study using: TG-DSC-IR, HSM-MS and GC-MS
    Nascimento, A. L. C. S.
    Ashton, G. P.
    Parkes, G. M. B.
    Ekawa, B.
    Fernandes, R. P.
    Carvalho, A. C. S.
    Ionashiro, M.
    Caires, F. J.
    JOURNAL OF ANALYTICAL AND APPLIED PYROLYSIS, 2019, 144
  • [47] Thermal Activation of Solid-State Molybdenum Halide Clusters with an Octahedral Cluster Framework and Their Application to Catalytic Synthesis of 3-Methylpyridine from Piperidine and Methanol
    Kamiguchi, Satoshi
    Kajio, Ryu
    Yamada, Hitomi
    Yuge, Hidetaka
    Okumura, Kazu
    Iida, Hajime
    Nagashima, Sayoko
    Chihara, Teiji
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 2015, 88 (08) : 1116 - 1122
  • [48] Emission Quenching and First Evidence of Tb3+-to-As5+ Charge Transfer in Terbium(III) Ion-Doped YVxAs1-xO4 Solid-State Solution
    Wujczyk, Marta
    Watras, Adam
    Boutinaud, Philippe
    Bettinelli, Marco
    Targonska, Sara
    Holsa, Jorma
    Wiglusz, Rafal J.
    JOURNAL OF PHYSICAL CHEMISTRY C, 2020, 124 (31) : 17364 - 17371
  • [49] Masking of Lewis acidity trends in the solid-state structures of trichlorido- and tribromido(2,2′:6′,2"-terpyridine-κ3N,N′,N")gallium(III)
    Kazakov, Igor V.
    Bodensteiner, Michael
    Timoshkin, Alexey Y.
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2014, 70 : 312 - U248
  • [50] Substituted oxetanes in polymer synthesis. III. Polyesters based on 3,3-bis(chloromethyl)oxetane and various dicarboxylates. The influence of the chemical structure upon thermal behaviour
    Bulacovschi, V
    Toader, V
    JOURNAL OF THE SERBIAN CHEMICAL SOCIETY, 1998, 63 (06) : 445 - 453
12345