Effects of heat treatment on the structural, spectral, morphological, dielectric, and magnetic properties of Ba0.5Sr0.1Zn0.4Fe12O19 ferrite

被引:9
作者
Shifa, Muhammad Shahzad [1 ]
Khan, Waqar Ahmed [2 ]
Albalawi, Hind [3 ]
Muhimeed, Tahani I. Al- [4 ]
AlObaid, Abeer A. [4 ]
Mahmood, Q. [5 ,6 ]
Khan, Muhammad Azhar [1 ]
Gulbadan, Shagufta [1 ]
Gilani, Zaheer Abbas [7 ]
Qureshi, Imdadullah [8 ]
机构
[1] Islamia Univ Bahawalpur, Inst Phys, Bahawalpur 63100, Pakistan
[2] Govt Coll Univ, Dept Phys, Nanaoferrites Synth & Texture Anal Lab, Faisalabad, Pakistan
[3] Princess Nourah Bint Abdulrahman Univ PNU, Coll Sci, Dept Phys, Riyadh 11671, Saudi Arabia
[4] King Saud Univ, Dept Chem, Coll Sci, POB 22452, Riyadh 11495, Saudi Arabia
[5] Imam Abdulrahman Bin Faisal Univ, Basic & Appl Sci Res Ctr, POB 1982, Dammam 31441, Saudi Arabia
[6] Imam Abdulrahman Bin Faisal Univ, Dept Phys, POB 1982, Dammam 31441, Saudi Arabia
[7] Balochistan Univ Informat Technol Engn & Manageme, Dept Phys, Quetta, Pakistan
[8] Univ Sci & Technol Bannu, Dept Chem, Bannu, Pakistan
关键词
M-type hexaferrite; XRD; SEM; FTIR; Dielectric characteristics; Magnetic characteristics; MICROWAVE-ABSORPTION; HEXAGONAL FERRITE; AC SUSCEPTIBILITY; NANO-POWDERS; HEXAFERRITES; SUBSTITUTION; MOSSBAUER; BEHAVIOR; SOFT; PR;
D O I
10.1016/j.ceramint.2021.05.207
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
M-type Hexa-ferrites powders of chemical composition Ba0.5Sr0.1Zn0.4Fe12O19 was prepared by the use of the coprecipitation technique. The heat treatment of this ferrite composition was done at various temperatures (700, 800, 900, 1000, 1100, and 1200 degrees C) for 6 h. The X-ray diffraction (XRD) analysis of all the prepared powder samples confirmed the emergence of a hexagonal structure. The high-intensity peaks of the samples were indexed and showed a single phase. The size of crystallite was obtained within the range of 21-42 nm. The surface morphology was carried out with a Scanning electron microscope (SEM). The grain size showed the hexagonal shape, and average grain sizes were in the range of similar to 211 nm. Spectral information was found using the Fourier transform infrared (FTIR) spectroscopy to confirm the phase of M-type hexaferrite. The dielectric parameters were measured within the high-frequency range of 5 MHz - 3 GHz. The dielectric constant was increased with an increase in temperature. The dielectric studies were found by the establishment of space charge polarization as per the two-layer model provided by Maxwell-Wagner and the study of phenomena of Koop's theory. The magnetic characteristics including coercivity (HcB) and retentivity (Br) were measured from BH/JH hysteresis loops. The enhancement of coercivity was observed from 1.23 x 10(+3) Oe to 1.50 x 10(+3) Oe, while the retentivity increased from 1.334 x 10(+3) G to 1.598 x 10(+3) G with an increase in temperature. Outstanding properties of synthesized materials suggested their use in large-frequency applications, including recording media and permanent magnets.
引用
收藏
页码:24817 / 24822
页数:6
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