An experimental method for the in situ observation of eutectic growth patterns in bulk samples of transparent alloys

被引:30
|
作者
Bottin-Rousseau, Sabine
perrut, Mikaeel
Picard, Christian
Akamatsu, Silvere
Faivre, Gabriel
机构
[1] Univ Paris 06, CNRS, UMR 7588, Inst Nanosci Paris, F-75015 Paris, France
[2] Univ Denis Diderot Paris 7, F-75015 Paris, France
关键词
eutectics; optical microscope; solidification; bridgman technique; growth from melt; transparent alloys;
D O I
10.1016/j.jcrysgro.2007.05.035
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
We present an experimental method for the in situ observation of directional-solidification fronts in bulk samples of transparent eutectic alloys. The growth front is observed obliquely in dark field through the liquid and a glass wall of the container with a longdistance microscope. We show that a focused image of the whole growth front can be obtained at a certain tilt angle of the microscope. At this tilt angle, eutectic fibers of about 3.5 mu m in diameter can be clearly seen over the whole growth front in 400 Pin thick samples. (c) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:465 / 472
页数:8
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