tert-Butylzinc hydroxide as an efficient predesigned precursor of ZnO nanoparticles

被引:37
作者
Bury, Wojciech [1 ]
Krajewska, Elzbieta [1 ]
Dutkiewicz, Michal [1 ]
Sokolowski, Kamil [2 ]
Justyniak, Iwona [2 ]
Kaszkur, Zbigniew [2 ]
Kurzydlowski, Krzysztof J. [3 ]
Plocinski, Tomasz [3 ]
Lewinski, Janusz [1 ,2 ]
机构
[1] Warsaw Univ Technol, Fac Chem, PL-00664 Warsaw, Poland
[2] Polish Acad Sci, Inst Phys Chem, PL-01224 Warsaw, Poland
[3] Warsaw Univ Technol, Fac Mat Sci & Engn, PL-02507 Warsaw, Poland
关键词
ZINC-OXIDE NANOPARTICLES; ATOMIC LAYER DEPOSITION; SENSITIZED SOLAR-CELLS; ORGANOMETALLIC CHEMISTRY; WATER; SIZE; ALKYLALUMOXANES; BUTYLALUMINUM; NANOCRYSTALS; DIETHYLZINC;
D O I
10.1039/c1cc11328c
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The reaction of (t)Bu(2)Zn with water was investigated which led to isolation of the novel hexameric tert-butylzinc hydroxide. The resulting zinc hydroxide cluster appears to be an ideal predesigned single-source precursor which decomposes smoothly in one step at only ca. 120 degrees C into ZnO nanoparticles.
引用
收藏
页码:5467 / 5469
页数:3
相关论文
共 31 条
[1]   Formation of the first aryl zinc-hydroxy cubane, [ArZn(OH)]4 (Ar=2,4,6-(CF3)3C6H2) [J].
Agnew, Caroline ;
Dillon, Keith B. ;
Goeta, Andres E. ;
Thompson, Amber L. .
INORGANICA CHIMICA ACTA, 2009, 362 (11) :4260-4262
[2]   NOVEL ALKYLMETAL HYDROXIDES - THE CRYSTAL AND MOLECULAR-STRUCTURES OF BIS(MU-HYDROXY)-BIS(TRIS(DIMETHYLPHENYLSILYL)METHYLZINC), [(ME2PHSI)3CZNOH)2] AND MU-4-OXOHEXA(MU-HYDROXY)TETRAKIS(TRIS(TRIMETHYLSILYL)METHYLINDIUM), [O((ME3SI)3CLN)4(OH)6] [J].
ALJUAID, SS ;
BUTTRUS, NH ;
EABORN, C ;
HITCHCOCK, PB ;
ROBERTS, ATL ;
SMITH, JD ;
SULLIVAN, AC .
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1986, (12) :908-909
[3]   Aerogel templated ZnO dye-sensitized solar cells [J].
Hamann, Thomas W. ;
Martinson, Alex B. E. ;
Elam, Jeffrey W. ;
Pellin, Michael J. ;
Hupp, Joseph T. .
ADVANCED MATERIALS, 2008, 20 (08) :1560-+
[4]   TERT-BUTYLALUMINUM HYDROXIDES AND OXIDES - STRUCTURAL RELATIONSHIP BETWEEN ALKYLALUMOXANES AND ALUMINA GELS [J].
HARLAN, CJ ;
MASON, MR ;
BARRON, AR .
ORGANOMETALLICS, 1994, 13 (08) :2957-2969
[5]   MECHANISMS OF REACTIONS OF DIETHYLZINC WITH ISOPROPANOL AND WATER [J].
HEROLD, RJ ;
NEFF, V ;
AGGARWAL, SL .
CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1963, 41 (05) :1368-&
[6]   Spontaneous formation of ordered 2D and 3D superlattices of ZnO nanocrystals [J].
Kahn, ML ;
Monge, M ;
Snoeck, E ;
Maisonnat, A ;
Chaudret, B .
SMALL, 2005, 1 (02) :221-224
[7]   Size- and shape-control of crystalline zinc oxide nanoparticles:: A new organometallic synthetic method [J].
Kahn, ML ;
Monge, M ;
Collière, V ;
Senocq, F ;
Maisonnat, A ;
Chaudret, B .
ADVANCED FUNCTIONAL MATERIALS, 2005, 15 (03) :458-468
[8]   Organometallic chemistry: an alternative approach towards metal oxide nanoparticles [J].
Kahn, Myrtil L. ;
Glaria, Arnaud ;
Pages, Carole ;
Monge, Miguel ;
Saint Macary, Lena ;
Maisonnat, Andre ;
Chaudret, Bruno .
JOURNAL OF MATERIALS CHEMISTRY, 2009, 19 (24) :4044-4060
[9]   Monodispersed ZnO nanoparticles from a single molecular precursor [J].
Kim, CG ;
Sung, KW ;
Chung, TM ;
Jung, DY ;
Kim, Y .
CHEMICAL COMMUNICATIONS, 2003, (16) :2068-2069
[10]   ETHYLZINC HYDROXIDE AS AN INTERMEDIATE IN THE REACTION OF DIETHYLZINC WITH WATER [J].
KURAN, W ;
CZERNECKA, M .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1984, 263 (01) :1-7