Synthesis of FeS Nanoparticles for the Catalytic Reduction of 2,4-Dinitrochlorobenzene

被引：3
作者：
Song, Y. Z. [1 ]
Zhang, W. [1 ]
Chen, J. [1 ]
Lu, Y. T. [1 ]
Song, J. [1 ]
Zhang, L. L. [1 ]
Xie, J. M. [2 ]
Ye, Y. [3 ]
机构：
[1] Huaiyin Normal Univ, Sch Chem & Chem Engn, Jiangsu Prov Key Lab Chem Low Dimens Mat, Huaian 223300, Peoples R China
[2] Jiangsu Univ, Sch Chem & Chem Engn, Zhenjiang 212013, Jiangsu, Peoples R China
[3] Hubei Univ, Sch Chem, Wuhan 430070, Peoples R China
来源：
RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY A | 2020年 / 94卷 / 06期
基金：
美国国家科学基金会;
关键词：
2; 4-dinitrochlorobenzene; FeS nano particles; CV; modified electrode;
D O I：
10.1134/S0036024420060266
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
The FeS nanoparticles have been synthesized from thioacetamide and ferric chloride by hydrothermal method, and the as-prepared nanoparticles have been characterized by X-ray diffraction, scanning electron microscopy, energy dispersive spectrometry and AC impedance spectrometry. Electrochemical reduction of 2,4-dinitrochlorobenzene at nano FeS-modified glassy carbon electrode is investigated, and the results indicating that the FeS have a certain catalytic effect on 2,4-dinitrochlorobenzene reduction. The reaction mechanism is also discussed.
引用
收藏
页码：1184 / 1189
页数：6
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共 11 条
  • [1] Factors controlling regioselectivity in the reduction of polynitroaromatics in aqueous solution
    Barrows, SE
    Cramer, CJ
    Truhlar, DG
    Elovitz, MS
    Weber, EJ
    [J]. ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1996, 30 (10) : 3028 - 3038
  • [2] Cathode potential regulation in a coupled bioelectrode-anaerobic sludge system for effective dechlorination of 2,4-dichloronitrobenzene
    Chen, Linlin
    Shao, Junjie
    Chen, Hui
    Wang, Caiqin
    Gao, Xinyi
    Xu, Xiangyang
    Zhu, Liang
    [J]. BIORESOURCE TECHNOLOGY, 2018, 254 : 180 - 186
  • [3] Oxidizing Impact Induced by Mackinawite (FeS) Nanoparticles at Oxic Conditions due to Production of Hydroxyl Radicals
    Cheng, Dong
    Yuan, Songhu
    Liao, Peng
    Zhang, Peng
    [J]. ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2016, 50 (21) : 11646 - 11653
  • [4] Mechano-thermal synthesis and characterization of nano-structured Fe/FeS for application in photocatalysis
    Esmaili, H.
    Sheibani, S.
    Rashchi, F.
    [J]. PARTICUOLOGY, 2018, 37 : 72 - 80
  • [5] Selective synthesis of FeS and FeS2 nanosheet films on iron substrates as novel photocathodes for tandem dye-sensitized solar cells
    Hu, Yan
    Zheng, Zhi
    Jia, Huimin
    Tang, Yiwen
    Zhang, Lizhi
    [J]. JOURNAL OF PHYSICAL CHEMISTRY C, 2008, 112 (33) : 13037 - 13042
  • [6] Highly Porous FeS/Carbon Fibers Derived from Fe-Carrageenan Biomass: High-capacity and Durable Anodes for Sodium-Ion Batteries
    Li, Daohao
    Sun, Yuanyuan
    Chen, Shuai
    Yao, Jiuyong
    Zhang, Yuhui
    Xia, Yanzhi
    Yang, Dongjiang
    [J]. ACS APPLIED MATERIALS & INTERFACES, 2018, 10 (20) : 17175 - 17182
  • [7] Enhancing As(V) adsorption and passivation using biologically formed nano-sized FeS coatings on limestone: Implications for acid mine drainage treatment and neutralization
    Liu, Jing
    Zhou, Lei
    Dong, Faqin
    Hudson-Edwards, Karen A.
    [J]. CHEMOSPHERE, 2017, 168 : 529 - 538
  • [8] Density functional theory study on electrochemical reduction of 2,4-dinitrophenol
    Song, Y. Z.
    [J]. RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY A, 2014, 88 (09) : 1550 - 1558
  • [9] Mechano-chemical processing and characterization of nano-structured FeS powder
    Soori, M.
    Zarezadeh, K.
    Sheibani, S.
    Rashchi, F.
    [J]. ADVANCED POWDER TECHNOLOGY, 2016, 27 (02) : 557 - 563
  • [10] FeS@C on Carbon Cloth as Flexible Electrode for Both Lithium and Sodium Storage
    Wei, Xiang
    Li, Weihan
    Shi, Jin-an
    Gu, Lin
    Yu, Yan
    [J]. ACS APPLIED MATERIALS & INTERFACES, 2015, 7 (50) : 27804 - 27809
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