Reciprocal space mapping and single-crystal scattering rods

被引:30
作者
Smilgies, DM [1 ]
Blasini, DR
Hotta, S
Yanagi, H
机构
[1] Cornell Univ, CHESS Ctr, Ithaca, NY 14853 USA
[2] Cornell Univ, Dept Chem & Biol Chem, Ithaca, NY 14853 USA
[3] Kyoto Inst Technol, Dept Polymer Sci & Engn, Sakyo Ku, Kyoto 6068585, Japan
[4] Kobe Univ, Fac Engn, Nada Ku, Kobe, Hyogo 6578501, Japan
关键词
grazing-incidence diffraction; scattering rods; reciprocal space mapping;
D O I
10.1107/S0909049505030815
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Reciprocal space mapping using a linear gas detector in combination with a matching Soller collimator has been applied to map scattering rods of well oriented organic microcrystals grown on a solid surface. Formulae are provided to correct image distortions in angular space and to determine the required oscillation range, in order to measure properly integrated scattering intensities.
引用
收藏
页码:807 / 811
页数:5
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