Magic Angle Spinning NMR Spectroscopy: A Versatile Technique for Structural and Dynamic Analysis of Solid-Phase Systems

被引：80

作者：

Poenova, Tatyana ^{[1
]}

Gupta, Rupal ^{[1
]}

Goldbourt, Amir ^{[2
]}

机构：

[1] Univ Delaware, Dept Chem & Biochem, Newark, DE 19716 USA

[2] Tel Aviv Univ, Sch Chem, IL-69978 Ramat Aviv, Israel

来源：

ANALYTICAL CHEMISTRY | 2015年 / 87卷 / 11期

基金：

美国国家卫生研究院; 美国国家科学基金会;

关键词：

NUCLEAR-MAGNETIC-RESONANCE; LITHIUM-ION BATTERIES; PROTEIN-STRUCTURE DETERMINATION; FULLY PROTONATED PROTEINS; FINE-STRUCTURE CONSTANTS; CHEMICAL-SHIFT TENSORS; X-RAY-DIFFRACTION; STATE O-17 NMR; IN-SITU; HIGH-RESOLUTION;

D O I：

10.1021/ac504288u

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Magic Angle Spinning (MAS) NMR spectroscopy is a powerful method for analysis of a broad range of systems, including inorganic materials, pharmaceuticals, and biomacromolecules. The recent developments in MAS NMR instrumentation and methodologies opened new vistas to atomic-level characterization of a plethora of chemical environments previously inaccessible to analysis, with unprecedented sensitivity and resolution.

引用

页码：5458 / 5469

页数：12

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