Magic-angle-spinning solid-state NMR applied to polypeptides and proteins

被引：19
|
作者：
Hughes, CE [1 ]
Baldus, M [1 ]
机构：
[1] Max Planck Inst Biophys Chem, Dept NMR Based Struct Bioil, D-37077 Gottingen, Germany
来源：
ANNUAL REPORTS ON NMR SPECTROSCOPY, VOL 55 | 2005年 / 55卷
关键词：
D O I：
10.1016/S0066-4103(04)55002-0
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
This chapter deals with the topic of polypeptide structure elucidation using the technique of magic-angle-spinning (MAS) solid-state NMR. We discuss various aspects of sample preparation and recent progress in establishing high-resolution conditions for MAS-based structural studies. Approaches for obtaining structural parameters in multiply or uniformly labelled polypeptides are reviewed. Recent applications to globular mid membrane-associated proteins are summarized.
引用
收藏
页码：121 / 158
页数：38
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