ANALYTICAL APPROACHES FOR SAMPLING AND SAMPLE PREPARATION FOR HEAVY METALS ANALYSIS IN BIOLOGICAL MATERIALS

被引：3

作者：

Chirila, Elisabeta ^{[1
]}

Draghici, Camelia ^{[2
]}

机构：

[1] Ovidius Univ Constanta, 124 Mamaia Blvd, Constanta 900527, Romania

[2] Transilvania Univ Brasov, Brasov 500036, Romania

来源：

ENVIRONMENTAL HEAVY METAL POLLUTION AND EFFECTS ON CHILD MENTAL DEVELOPMENT: RISK ASSESSMENT AND PREVENTION STRATEGIES | 2010年

关键词：

Heavy metals; sampling; biological sample preparation; speciation; BLOOD LEAD LEVELS; HUMAN WHOLE-BLOOD; GAS-CHROMATOGRAPHY; CHILDREN; URINE; SPECIATION; PLASMA; EXTRACTION; MANGANESE; CADMIUM;

D O I：

10.1007/978-94-007-0253-0_8

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

Heavy metals concentrations in biological materials are necessary to be known when investigations in environmental or health risk assessment are done. The paper aims to review the modern aspects of the first step of the analytical process, sampling and sample preparation which involve some of the following operations: sample collection (sampling), washing, storage, preservation, followed by sample transformation to the most appropriate form for measurement. New separation techniques, applied for specific analytes extraction or preconcentration from biological matrices and metal speciation are also briefly described.

引用

页码：129 / +

页数：4

共 34 条

[1] Biomonitoring of manganese in blood, urine and axillary hair following low-dose exposure during the manufacture of dry cell batteries [J].

Bader, M ;

Dietz, MC ;

Ihrig, A ;

Triebig, G .

INTERNATIONAL ARCHIVES OF OCCUPATIONAL AND ENVIRONMENTAL HEALTH, 1999, 72 (08) :521-527

[2] Blood and urine levels of Pb, Cd and Hg in the general population of the Czech Republic and proposed reference values [J].

Batariova, Andrea ;

Spevackova, Vera ;

Benes, Bohuslav ;

Cejchanova, Maja ;

Smid, Jiri ;

Cerna, Milena .

INTERNATIONAL JOURNAL OF HYGIENE AND ENVIRONMENTAL HEALTH, 2006, 209 (04) :359-366

[3]

Borosová D, 2008, CARPATH J EARTH ENV, V3, P23

[4] SPECIATION OF MERCURY IN HUMAN WHOLE-BLOOD BY CAPILLARY GAS-CHROMATOGRAPHY WITH A MICROWAVE-INDUCED PLASMA EMISSION DETECTOR SYSTEM FOLLOWING COMPLEXOMETRIC EXTRACTION AND BUTYLATION [J].

BULSKA, E ;

EMTEBORG, H ;

BAXTER, DC ;

FRECH, W ;

ELLINGSEN, D ;

THOMASSEN, Y .

ANALYST, 1992, 117 (03) :657-663

[5] Exposure to arsenic and lead of children living near a copper-smelter in San Luis Potosi, Mexico:: Importance of soil contamination for exposure of children [J].

Carrizales, L ;

Razo, I ;

Téllez-Hernández, JI ;

Torres-Nerio, R ;

Torres, A ;

Batres, LE ;

Cubillas, AC ;

Díaz-Barriga, F .

ENVIRONMENTAL RESEARCH, 2006, 101 (01) :1-10

[6] Sampling and sample pretreatment for environmental analysis [J].

Chirila, Elisabeta S. ;

Draghici, Camelia ;

Dobrinas, Simona .

CHEMICALS AS INTENTIONAL AND ACCIDENTAL GLOBAL ENVIRONMENTAL THREATS, 2006, :7-+

[7] Direct analysis of human blood (mothers and newborns) by energy dispersive X-ray fluorescence [J].

Custódio, PJ ;

Carvalho, ML ;

Nunes, F ;

Pedroso, S ;

Campos, A .

JOURNAL OF TRACE ELEMENTS IN MEDICINE AND BIOLOGY, 2005, 19 (2-3) :151-158

[8]

DRAGHICI C, 2010, ANAL SEPARATION METH

[9]

FATIMA RM, 2007, INT J HYG ENVIR HEAL, V210, P439

[10]

FATIMA RM, 2007, J HYG ENV HLTH, V210, P447

← 1 2 3 4 →