Synthesis of 2-(halomethyl)-3,4-dihydro-2H-pyrido[2,1-b][1,3]oxazinium halides

被引：1

作者：

Kalita, E. V. ^{[1
]}

Kim, D. G. ^{[1
]}

机构：

[1] South Ural State Univ, Pr Lenina 76, Chelyabinsk 454080, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2017年 / 53卷 / 07期

关键词：

DERIVATIVES;

D O I：

10.1134/S1070428017070132

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Alkylation of pyridin-2(1H)-one and 5-nitropyridin-2(1H)-one with 4-bromobut-1-ene afforded a mixture of N- and O-butenyl derivatives. 1-(But-3-en-1yl)pyridin-2(1H)-one and 1-(but-3-en-1-yl)-5-nitropyridin- 2(1H)-one reacted with bromine and iodine to give 2-(halomethyl)-3,4-dihydro-2H-pyrido[2,1-b][1,3]-oxazinium halides.

引用

页码：1040 / 1043

页数：4

共 8 条

[1] ANTIBACTERIAL ACTIVITY OF DIHYDRO-1,3-OXAZINE DERIVATIVES CONDENSED WITH AROMATIC RINGS IN POSITIONS 5,6
CHYLINSKA, JB
JANOWIEC, M
URBANSKI, T
[J]. BRITISH JOURNAL OF PHARMACOLOGY, 1971, 43 (03) : 649 - +
[2] Czarnik AW, 1996, ACCOUNTS CHEM RES, V29, P112, DOI 10.1021/ar950256n
[3] A Practical Route for the Preparation of 1,4,7-Triazacyclononanyl Diacetates with a Hydroxypyridinonate Pendant Arm
Gai, Yongkang
Hu, Zhongping
Rong, Zhao
Ma, Xiang
Xiang, Guangya
[J]. MOLECULES, 2015, 20 (10) : 19393 - 19405
[4] Alkenyl Derivatives of 5-Nitro-2-pyridone: Synthesis and Halocyclization
Kalita, E. V.
Kim, D. G.
Yeltsov, O. S.
Shtukina, T. S.
[J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2016, 52 (08) : 1148 - 1153
[5] MESOIONIC 6-MEMBERED HETEROCYCLES .11. SYNTHESIS AND REACTIONS OF MESOIONIC 1,3-OXAZINES
KAPPE, T
GOLSER, W
HARIRI, M
STADLBAUER, W
[J]. CHEMISCHE BERICHTE-RECUEIL, 1979, 112 (05): : 1585 - 1594
[6] Kim D.G., 2012, VESTN YUZHNO URAL K, V24, P13
[7] Preparation of Heteroaryl Ethers from Azine N-Oxides and Alcohols
Lian, Yajing
Coffey, Steven B.
Li, Qifang
Londregan, Allyn T.
[J]. ORGANIC LETTERS, 2016, 18 (06) : 1362 - 1365
[8] UMSETZUNGEN DES ALPHA-PYRIDONS
WINTERFELD, K
MICHAEL, H
[J]. CHEMISCHE BERICHTE-RECUEIL, 1960, 93 (01): : 61 - 64

← 1 →