A gas chromatography quartz crystal microbalance for speciation of nitroaromatic compounds in landfill gas

被引:4
作者
Santos, TAPR [1 ]
Duarte, AC [1 ]
Oliveira, JABP [1 ]
机构
[1] Univ Aveiro, Dept Chem, P-3810193 Aveiro, Portugal
关键词
nitroaromatic compounds; speciation; landfill gas; quartz crystal microbalance;
D O I
10.1016/S0039-9140(00)00670-6
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A new method based on separation with gas chromatography and detection with a quartz crystal microbalance was used for quantification of nitrobenzene, 2-. 3- and 4-nitrotoluene in landfill gas. The analytical error? the analysis time and general analytical performance were identical for gas chromatography-mass spectrometry (GC-MS) and gas chromatography-quartz crystal microbalance (GC-QCM). GC-QCM constitutes a very inexpensive alternative to GC-MS for monitoring nitroaromatic compounds in landfill gas. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:383 / 388
页数:6
相关论文
共 14 条
[1]   Application of piezoelectric Ru(III)/cryptand-coated quartz crystal gas chromatographic detector for olefins [J].
Chang, P ;
Shih, JS .
ANALYTICA CHIMICA ACTA, 1999, 380 (01) :55-62
[2]   Preparation and application of cryptand-coated piezoelectric crystal gas-chromatographic detector [J].
Chang, P ;
Shih, JS .
ANALYTICA CHIMICA ACTA, 1998, 360 (1-3) :61-68
[3]  
CHRISTENSEN TH, 1996, LANDFILLING WASTE BI, P51
[4]   SURFACE-ENHANCED RAMAN-SPECTROSCOPY AS A PROBE OF ADSORBATE SURFACE BONDING - BENZENE AND MONOSUBSTITUTED BENZENES ADSORBED AT GOLD ELECTRODES [J].
GAO, P ;
WEAVER, MJ .
JOURNAL OF PHYSICAL CHEMISTRY, 1985, 89 (23) :5040-5046
[5]   GAS-CHROMATOGRAPHIC DETECTOR FOR SELECTIVE AND SENSITIVE DETECTION OF ATMOSPHERIC ORGANIC NITRATES [J].
HAO, CS ;
SHEPSON, PB ;
DRUMMOND, JW ;
MUTHURAMU, K .
ANALYTICAL CHEMISTRY, 1994, 66 (21) :3737-3743
[6]  
*JAND SCI, 1994, SIGM STAT STAT SOFTW
[7]  
JANGHORB.M, 1973, ANAL CHEM, V45, P325, DOI 10.1021/ac60324a040
[8]   CHROMATOGRAPHIC DESIGN AND TEMPERATURE-RELATED CHARACTERISTICS OF PIEZOELECTRIC DETECTOR [J].
KARASEK, FW ;
GUY, P ;
HILL, HH ;
TIERNAY, JM .
JOURNAL OF CHROMATOGRAPHY, 1976, 124 (02) :179-186
[9]   GAS CHROMATOGRAPH BASED ON PIEZOELECTRIC DETECTOR [J].
KARASEK, FW ;
GIBBINS, KR .
JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1971, 9 (09) :535-+
[10]   PIEZOELECTRIC SORPTION DETECTOR [J].
KING, WH .
ANALYTICAL CHEMISTRY, 1964, 36 (09) :1735-&