N′-(3,4-Dimethoxybenzylidene)-3,5-dihydroxybenzohydrazide methanol monosolvate

被引：0

作者：

Zhang, Qi-Hui ^{[1
]}

Zhou, Lian-Di ^{[2
]}

Li, Chuan-Xun ^{[3
]}

Huang, Shan-Shan ^{[3
]}

Zhang, Bao-Jing ^{[3
]}

机构：

[1] Chongqing Univ, Coll Chem & Chem Engn, Chongqing 400030, Peoples R China

[2] Chongqing Med Univ, Basic Med Coll, Dept Immunol, Chongqing 400016, Peoples R China

[3] Dalian Med Univ, Sch Pharm, Dalian 116044, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷

关键词：

data-to-parameter ratio = 12.6; mean σ(CC) = 0.003 Å; R factor = 0.055; single-crystal X-ray study; T = 295 K; wR factor = 0.162;

D O I：

10.1107/S1600536811029850

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C16H16N2O5 center dot CH4O, the two benzene rings in the Schiff base molecule form a dihedral angle of 17.1 (1)degrees. In the crystal, intermolecular O-H center dot center dot center dot O hydrogen bonds link the components into corrugated sheets parallel to the (101) plane.

引用

页码：O2189 / U1905

页数：9

共 50 条

[31] catena-Poly[[[dichloridomercury(II)]-μ-1,4-bis(3-pyridylaminomethyl) benzene-κ2N:N'] N,N-dimethylformamide monosolvate] [J].

Gao, Shan ;

Ng, Seik Weng .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :M1051-U504

[32] (E)-N'-(2-Hydroxy-3,5-diiodobenzyl-idene)-3- methylbenzohydrazide [J].

Tang, Chun-Bao .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O603-U1405

[33] N-[2-(3,4-Dimethoxyphenyl) ethyl]N-methylnaphthalene-1-sulfonamide [J].

Vennila, Jasmine P. ;

Thiruvadigal, D. John ;

Kavitha, Helen P. ;

Chakkaravarthi, G. ;

Manivannan, V. .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O890-U3318

[34] Carbonyl(η5-cyclopentadienyl)(3,5-dimethyl-pyridine-κN)(triethylsilyl)iron(II) [J].

Itazaki, Masumi ;

Ueda, Kensuke ;

Nakazawa, Hiroshi .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 :M1312-M1313

[35] Diethyl 2,5-bis[(2,3-dihydrothieno[3,4-b][1,4]dioxin-5-yl) methylideneamino]thiophene-3,4-dicarboxylate acetone monosolvate [J].

Dufresne, Stephane ;

Bolduc, Andreanne ;

Skene, W. G. .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O3138-U1736

[36] 4-[3,5-Bis(2-hydroxyphenyl)-1H-1,2,4-triazol-1-yl]benzoic acid dimethyl-formamide monosolvate [J].

Fun, Hoong-Kun ;

Chantrapromma, Suchada ;

Dayananda, A. S. ;

Yathirajan, H. S. ;

Thomas, Saji .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 :O792-U2649

[37] 2-Methoxy-N-[(S)-3-methylbutan-2-yl]-6-{[(S)-3-methylbutan-2-yl]amino}-3,5-dinitrobenzamide [J].

Wu, Xuefen ;

Chen, Xi ;

Hou, Yimin .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O3482-U1647

[38] (E)-5-(3,5-Dimethylphenyl)-N-[4-(methylsulfanyl)benzylidene]-1,3,4-thiadiazol-2-amine [J].

Hu, Jun ;

Ji, Jin-xiu ;

Zhou, Ying ;

Wang, Ji-kui ;

Xu, Yan-hua .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :O410-U2924

[39] N′-[6-(3,5-Dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazin-3-yl]butanohydrazide [J].

Yan, Qi-Dong ;

Xu, Feng ;

Xu, Jun .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 :O3339-U1004

[40] Bis[(1-methyl-1H-benzimidazol-2-yl)methanol-κ2N3,O]bis(thiocyanato-κN)cobalt(II) methanol solvate [J].

Zhou, Yan-Ling ;

Liang, Hong ;

Zeng, Ming-Hua .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 :M189-U963

← 1 2 3 4 5 →