An in-situ TEM characterization of electron beam induced dislocation motion in a single-crystalline gold thin film

被引:3
作者
Xu, Chi [1 ,3 ,4 ]
Han, Wentuo [2 ]
Xue, Wenbin [1 ,3 ]
Li, Yongliang [4 ]
Li, Song [4 ]
Li, Bingsheng [5 ]
Wan, Farong [2 ]
机构
[1] Beijing Normal Univ, Coll Nucl Sci & Technol, Key Lab Beam Technol, Minist Educ, Beijing 100875, Peoples R China
[2] Univ Sci & Technol Beijing, Dept Mat Phys, Beijing 100086, Peoples R China
[3] Beijing Radiat Ctr, Beijing 100875, Peoples R China
[4] Beijing Normal Univ, Analyt & Testing Ctr, Beijing 100875, Peoples R China
[5] Southwest Univ Sci & Technol, State Key Lab Environm Friendly Energy Mat, Mianyang 621010, Sichuan, Peoples R China
基金
中国国家自然科学基金;
关键词
In-situ; TEM characterization; Dislocation motion; Au crystal; Stacking fault; STACKING-FAULT ENERGY; AUSTENITIC STAINLESS-STEEL; IRRADIATION DAMAGE; DEFORMATION MICROSTRUCTURES; TEMPERATURE-DEPENDENCE; GLIDE; GAAS; MICROSCOPY; BICRYSTALS; METALS;
D O I
10.1016/j.matchar.2021.111697
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Dislocation motions driven by electron-beam illumination were in-situ observed in a single-crystalline gold thinfoil specimen, under a medium-voltage transmission electron microscope operated at 200 kV. The dislocation motion characteristics were in-situ observed under the bright-field and weak-beam dark-field conditions. The structures formed through the dislocation motion were also characterized using bright-/dark-field imaging and high-resolution techniques. Two types of dislocation motions are concluded, where one type of motion left no apparent traces, and the other type left a clear trace of passage. The dislocation motions have jerky behaviors, and the motions are accelerated when the beam intensity is increased. The immobile trace structures left by the dislocation motions are identified to be twin structures oriented along the < 111 > crystal directions. The dislocation motion mechanism is discussed and the motion might be caused by the electron beam heating effect or the electron beam induced phonon effects. The dislocation disassociation, planar defect formation in the Au crystal, and the beam heating impacts are also discussed.
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页数:9
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