Analysis of the Electroconsolidation Process of Fine-Dispersed Structures Out of Hot Pressed Al2O3WC Nanopowders

被引:16
作者
Gevorkyan, Edwin [1 ]
Rucki, Miroslaw [2 ]
Krzysiak, Zbigniew [3 ]
Chishkala, Volodymyr [4 ]
Zurowski, Wojciech [2 ]
Kucharczyk, Wojciech [2 ]
Barsamyan, Voskan [5 ]
Nerubatskyi, Volodymyr [1 ]
Mazur, Tomasz [2 ]
Morozow, Dmitrij [2 ]
Siemiatkowski, Zbigniew [2 ]
Caban, Jacek [6 ]
机构
[1] Ukraine State Univ Railway Transport, Wagon Engn & Prod Qual, 7 Feuerbach Sq, UA-61010 Kharkiv, Ukraine
[2] Kazimierz Pulaski Univ Technol & Humanities Radom, Fac Mech Engn, Stasieckiego 54, PL-26600 Radom, Poland
[3] Univ Life Sci Lublin, Fac Prod Engn, Gleboka 28, PL-20612 Lublin, Poland
[4] Kharkov Natl Univ, Dept Reactor Engn Mat & Phys Technol, 4 Svobody Sq, UA-61022 Kharkiv, Ukraine
[5] Natl Polytech Univ Armenia, Vanadzor Branch, Chair Appl Phys, Vanadzor 2011, Armenia
[6] Lublin Univ Technol, Fac Mech Engn, Nadbystrzycka 36, PL-20618 Lublin, Poland
关键词
electroconsolidation; nanopowder; tungsten carbide; fast sintering; grain growth; diffusion; WEAR BEHAVIOR; COATINGS; MICROSTRUCTURE; COMPACTION; COMPOSITE; EVOLUTION; POWDER; IMPACT;
D O I
10.3390/ma14216503
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Fabrication of alumina-tungsten carbide nanocomposite was investigated. Characteristics of the densification and sintering were analyzed considering both the nano-size particle starting powders and the processing stages. Different heating rates were generated during densification and consolidation with a maximal load was applied only after a temperature of 1000 & DEG;C was reached. Due to the varying dominance of different physical processes affecting the grains, appropriate heating rates and pressure at different stages ensured that a structure with submicron grains was obtained. With directly applied alternating current, it was found that the proportion Al2O3 (50 wt.%)-WC provided the highest fracture toughness, and a sintering temperature above 1600 & DEG;C was found to be disadvantageous. High heating rates and a short sintering time enabled the process to be completed in 12 min, saving energy and time.
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页数:14
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