A new synchrotron-based diffraction technique for perturbation crystallography

被引:8
作者
Graafsma, H
Heunen, GWJC
Schulze, C
机构
[1] European Synchrotron Radiat Facil, F-38043 Grenoble, France
[2] Paul Scherrer Inst, Swiss Light Source Project, CH-5232 Villigen, Switzerland
关键词
D O I
10.1107/S0021889897014933
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A new diffraction technique based on a wide-energy-bandpass X-ray beam in connection with lock-in detection for diffraction studies of crystals subjected to external perturbations has been developed. The broad-energy-bandpass beam is obtained by combining a wiggler or bending-magnet source with a curved Si monochromator in Laue geometry. This new technique has been applied in diffraction experiments on single crystals in external electric fields. Both the speed and accuracy of the measurements are increased by more than two orders of magnitude compared with conventional methods.
引用
收藏
页码:414 / 422
页数:9
相关论文
共 15 条
  • [1] STRUCTURE RELATIONSHIP TO DIELECTRIC, ELASTIC AND CHIRAL PROPERTIES
    ABRAHAMS, SC
    [J]. ACTA CRYSTALLOGRAPHICA SECTION A, 1994, 50 : 658 - 685
  • [2] DEDXS - THE DIFFERENTIAL ENERGY-DISPERSIVE X-RAY SPECTROSCOPY SYSTEM AND ITS USE IN ELECTRIC-FIELD MODULATION STUDIES
    ADDISON, GT
    COUSINS, CSG
    FLOOD, SM
    HAMICHI, M
    MEADS, RE
    MINERS, F
    SHELDON, BJ
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1995, 97 (1-4) : 543 - 546
  • [3] DYNAMICAL X-RAY PROPAGATION - A THEORETICAL APPROACH TO THE CREATION OF NEW WAVE FIELDS
    BALIBAR, F
    CHUKHOVSKII, FN
    MALGRANGE, C
    [J]. ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (MAY): : 387 - 399
  • [4] X-RAY-DIFFRACTION CHARACTERISTICS OF CURVED MONOCHROMATORS FOR SYNCHROTRON RADIATION
    BOEUF, A
    LAGOMARSINO, S
    MAZKEDIAN, S
    MELONE, S
    PULITI, P
    RUSTICHELLI, F
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1978, 11 (OCT) : 442 - 449
  • [5] Phase objects in synchrotron radiation hard x-ray imaging
    Cloetens, P
    Barrett, R
    Baruchel, J
    Guigay, JP
    Schlenker, M
    [J]. JOURNAL OF PHYSICS D-APPLIED PHYSICS, 1996, 29 (01) : 133 - 146
  • [6] IMPLEMENTATION OF DEDXS - A DIFFERENTIAL ENERGY-DISPERSIVE X-RAY SPECTROSCOPY SYSTEM
    COUSINS, CSG
    HAMICHI, M
    MEADS, RE
    MINERS, F
    SHELDON, BJ
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1994, 345 (02) : 385 - 392
  • [7] ELECTRIC-FIELD-INDUCED IONIC DISPLACEMENT AND REDISTRIBUTION OF BONDING ELECTRONS IN LINBO3 AND LITAO3 REVEALED BY MODULATION X-RAY-DIFFRACTION
    FUJIMOTO, I
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 1982, 38 (MAY): : 337 - 345
  • [8] MOLECULAR-REORIENTATION IN AN ELECTRIC-FIELD AS STUDIED BY SINGLE-CRYSTAL X-RAY-DIFFRACTION
    GRAAFSMA, H
    PATURLE, A
    WU, L
    SHEU, HS
    MAJEWSKI, J
    POORTHUIS, G
    COPPENS, P
    [J]. ACTA CRYSTALLOGRAPHICA SECTION A, 1992, 48 : 113 - 120
  • [9] Wide dynamic range germanium detector for perturbation crystallography
    Graafsma, H
    Thorander, P
    Heunen, GWJC
    Morse, J
    [J]. JOURNAL OF SYNCHROTRON RADIATION, 1996, 3 : 156 - 159