Synthesis and Characterization of Nickel Oxide Nanostructures by Hydrothermal Method

被引:5
作者
Sathisha, D. [1 ]
Naik, K. Gopalakrishna [1 ]
机构
[1] Mangalore Univ, Dept Studies Phys, Mangalagangothri 574199, India
关键词
Nanostructures; Hydrothermal; Nanowire; Characterization; GAS-SENSING PROPERTIES; FLOWER-LIKE NIO; THIN-FILM; NANOSHEETS; PERFORMANCE; NANOPARTICLES; TEMPERATURE; ELECTRODES; SUPERCAPACITORS; BETA-NI(OH)(2);
D O I
10.1166/asl.2018.12178
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
Nickel oxide (NiO) nanostructures were synthesized by hydrothermal method using ethylene glycol and double distilled water as solvent in 3:2 volume ratio. The synthesized nanostructures were characterized by XRD, FESEM, EDX, FTIR, and UV-visible spectroscopy. XRD result shows that the synthesized nanostructures are polycrystalline in nature. FESEM images show the growth of NiO nanowires. The elemental compositions of the samples were analyzed by EDS. Fourier transform infrared (FTIR) spectroscopy confirms the existence of Ni-O bond in the sample. Optical band gap energy of about 3.71 eV was calculated from the UV-visible absorption measurement.
引用
收藏
页码:5691 / 5694
页数:4
相关论文
共 46 条
[41]  
Wen Z., 2012, T NONFERR METAL SOC, V22, P100
[42]  
Yao Y, 2012, INT J ELECTROCHEM SC, V7, P1433
[43]  
Yu L., 2015, APPL SURF SCI, V328, P525
[44]   Synthesis of porous NiO nanocrystals with controllable surface area and their application as supercapacitor electrodes [J].
Zhang, Xiaojun ;
Shi, Wenhui ;
Zhu, Jixin ;
Zhao, Weiyun ;
Ma, Jan ;
Mhaisalkar, Subodh ;
Maria, Tuti Lim ;
Yang, Yanhui ;
Zhang, Hua ;
Hng, Huey Hoon ;
Yan, Qingyu .
NANO RESEARCH, 2010, 3 (09) :643-652
[45]   Study of Schottky contact between Au and NiO nanowire by conductive atomic force microscopy (C-AFM): The case of surface states [J].
Zhang, Yidong .
PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES, 2015, 69 :109-114
[46]   Enhanced ethanol sensing performance of porous ultrathin NiO nanosheets with neck-connected networks [J].
Zhao, Changhui ;
Fu, Jiecai ;
Zhang, Zhenxing ;
Xie, Erqing .
RSC ADVANCES, 2013, 3 (12) :4018-4023