Synthesis of the pentasaccharide hapten from the glycopeptidolipid antigen of Mycobacterium avium serovar 17

被引：15
作者：
Varga, Z
Bajza, I
Batta, G
Lipták, A
机构：
[1] Univ Debrecen, Dept Biochem, H-4010 Debrecen, Hungary
[2] Hungarian Acad Sci, Res Grp Carbohydrates, H-4010 Debrecen, Hungary
[3] Hungarian Acad Sci, Res Grp Antibiot, H-4010 Debrecen, Hungary
来源：
TETRAHEDRON LETTERS | 2001年 / 42卷 / 31期
基金：
新加坡国家研究基金会; 匈牙利科学研究基金会;
关键词：
oligosaccharide; block synthesis; M. avium serovar 17; nilic acid; hapten; linker;
D O I：
10.1016/S0040-4039(01)00934-0
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Effective synthesis of the pentasaccharide hapten from the glycopeptidolipid antigen of Mycobacterium avium serovar 17 in a p-aminophenyl linker-containing form, using 3+2 block synthesis strategy, is described. A 2+3 block synthesis could not be achieved, although different glycosyl donors (1-Br, 1-SPh, 1-O-C(NH)CCl3) were used. (C) 2001 Elsevier Science Ltd. All rights reserved.
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页码：5283 / 5286
页数：4
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