A Macroscale Model for Hands-On Activities Demonstrating Transmission Electron Microscopy

被引:5
作者
Hudson-Smith, Natalie, V [1 ]
Cahill, Meghan S. [1 ]
Klein, Nathan D. [2 ]
Krause, Miriam O. P. [1 ]
Haynes, Christy L. [1 ]
机构
[1] Univ Minnesota, Dept Chem, 207 Pleasant St SE, Minneapolis, MN 55455 USA
[2] MIT, 77 Massachusetts Ave, Cambridge, MA 02139 USA
基金
美国国家科学基金会;
关键词
Nanotechnology; First-Year Undergraduate/General; Demonstrations; Hands-On Learning/Manipulatives; Materials Science; Analogies/Transfer; Instrumental Methods; NANOTECHNOLOGY; UNDERGRADUATE; FLUORESCENCE;
D O I
10.1021/acs.jchemed.8b01059
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Although nanotechnology lessons are increasingly integrated into curricula, students still face significant challenges in understanding the characterization techniques used to investigate nanotechnology. Many characterization techniques, such as transmission electron microscopy (TEM), are prohibitively expensive for primarily undergraduate institutions and completely inaccessible for high schools and local outreach programs. When TEMs are accessible, opportunities for hands-on use are still limited due to logistics and costs for instrument time. In this project, we present a low cost ($50 USD) macroscale TEM model that uses cyanotype paper for "imaging" and is constructed of materials available at local hardware and pet supply stores and chemistry stockrooms. This model allows students to investigate properties of TEM micrographs including thickness contrast, diffraction contrast, plan view, and tilt series imaging through a series of four hands-on activities in an active-learning setting. The four activities are identification of mystery objects from student cyanotype "micrographs", sizing objects from their micrographs using a scale bar, sketching the structure of a mystery 3D object from acquired tilt series images, and developing unique micrographs with objects of the students' choice and predicting features of the resulting images. The TEM model and associated activities were tested with groups of STEM (Science, Technology, Engineering and Mathematics)-interested high schoolers and were found to enhance student engagement, enjoyment, and understanding of certain properties of TEM micrographs.
引用
收藏
页码:1377 / 1382
页数:11
相关论文
共 50 条
  • [41] Targeted Ultramicrotomy: A Valuable Tool for Correlated Light and Electron Microscopy of Small Model Organisms
    Kolotuev, Irina
    Bumbarger, Daniel J.
    Labouesse, Michel
    Schwab, Yannick
    CORRELATIVE LIGHT AND ELECTRON MICROSCOPY, 2012, 111 : 203 - 222
  • [42] Revealing the heterogeneous contamination process in metal nanoparticulate catalysts in CO gas without purification by in situ environmental transmission electron microscopy
    Uchiyama, Tetsuya
    Yoshida, Hideto
    Kamiuchi, Naoto
    Kohno, Hideo
    Takeda, Seiji
    MICROSCOPY, 2016, 65 (06) : 522 - 526
  • [43] High-Resolution Scanning Transmission Electron Microscopy (HRSTEM) Techniques: High-Resolution Imaging and Spectroscopy Side by Side
    Stroppa, Daniel G.
    Zagonel, Luiz F.
    Montoro, Luciano A.
    Leite, Edson R.
    Ramirez, Antonio J.
    CHEMPHYSCHEM, 2012, 13 (02) : 437 - 443
  • [44] Cryo-transmission electron microscopy reveals mesoscopic H- and J-aggregates of near infrared cyanine dyes
    v. Berlepsch, Hans
    Boettcher, Christoph
    JOURNAL OF PHOTOCHEMISTRY AND PHOTOBIOLOGY A-CHEMISTRY, 2010, 214 (01) : 16 - 21
  • [45] Structural imaging of β-Si3N4 by spherical aberration-corrected high-resolution transmission electron microscopy
    Zhang, Zaoli
    Kaiser, Ute
    ULTRAMICROSCOPY, 2009, 109 (09) : 1114 - 1120
  • [46] Structure Prediction of Self-Assembled Dye Aggregates from Cryogenic Transmission Electron Microscopy, Molecular Mechanics, and Theory of Optical Spectra
    Friedl, Christian
    Renger, Thomas
    Berlepsch, Hans V.
    Ludwig, Kai
    Busch, Marcel Schmidt Am
    Megow, Joerg
    JOURNAL OF PHYSICAL CHEMISTRY C, 2016, 120 (34) : 19416 - 19433
  • [47] Interactions between DNA and a Pyrene-Labeled Surfactant Probed by Pyrene Excimer Formation, Transmission Electron Microscopy, and Dynamic Light Scattering
    Lloyd, Ryan
    Ba Salem, Abdullah
    Gallant, Noah
    Duhamel, Jean
    LANGMUIR, 2025, 41 (06) : 3768 - 3778
  • [48] In situ transmission electron microscopy of crystal growth-mode transitions during rapid solidification of a hypoeutectic Al-Cu alloy
    McKeown, Joseph T.
    Kulovits, Andreas K.
    Liu, Can
    Zweiacker, Kai
    Reed, Bryan W.
    LaGrange, Thomas
    Wiezorek, Joerg M. K.
    Campbell, Geoffrey H.
    ACTA MATERIALIA, 2014, 65 : 56 - 68
  • [49] Interaction of Localized Surface Plasmons of a Silver Nanosphere Dimer Embedded in a Uniform Medium: Scanning Transmission Electron Microscopy Electron Energy-Loss Spectroscopy and Discrete Dipole Approximation Simulation
    Sakaguchi, Norihito
    Matsumoto, Shuji
    Kunisada, Yuji
    Ueda, Mikito
    JOURNAL OF PHYSICAL CHEMISTRY C, 2019, 123 (11) : 6735 - 6744
  • [50] A New Geometric Method Based on Two-Dimensional Transmission Electron Microscopy for Analysis of Interior versus Exterior Pd Loading on Hollow Carbon Nanofibers
    Shuai, Danmeng
    Wang, Chongmin
    Genc, Arda
    Werth, Charles J.
    JOURNAL OF PHYSICAL CHEMISTRY LETTERS, 2011, 2 (09): : 1082 - 1087