Influence of the Mole Ratio, Sintering Condition and Particle Size on the Magnetic Properties of BaFe12O19 Synthesized by Ceramic Method

被引:13
作者
El-Lawindy, A. M. Y. [1 ]
Mansour, S. A. [1 ]
Hafiz, Mohamed [1 ]
Hassan, H. H. [2 ]
Ali, A. A. [1 ,3 ]
机构
[1] Suez Canal Univ, Dept Phys, Fac Sci, Ismailia, Egypt
[2] Cairo Univ, Fac Sci, Dept Phys, Giza, Egypt
[3] Sanaa Univ, Dept Phys, Fac Sci, Sanaa, Yemen
关键词
BARIUM; NANOPARTICLES; STRONTIUM;
D O I
10.1111/j.1744-7402.2009.02398.x
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Barium ferrite (BaFe12O19) with different particle sizes were successfully synthesized by solid-state reaction (ceramic method) using locally available low cost alpha-Fe2O3 mixed with BaO2. The prepared samples were sintered in the temperature range of 950 degrees to 1200 degrees C for 1.5 to 6 h. The prepared products of barium ferrite were characterized by X-ray diffraction, a scanning electron microscope, and a vibrating sample magnetometer. The effect of mole ratio, sintering temperature, and time was studied. A further addition of 10% BaO2 to the mole ratio (BaO2:5.7Fe(2)O(3)), and removing the particle size <63 mu m, exhibits a pure phase BaFe12O19. The saturation magnetization reached the optimum value of M-s= similar to 67 emu/g with coercivity of 2596 Oe, under sintering temperature up to 1100 degrees C for 4.5 h.
引用
收藏
页码:868 / 873
页数:6
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