A highly sensitive and ecofriendly assay platform for the simultaneous electrochemical determination of rifampicin and isoniazid in human serum and pharmaceutical formulations

被引：8

作者：

Sharafi, Effat ^{[1
]}

Sadeghi, Susan ^{[1
]}

机构：

[1] Univ Birjand, Dept Chem, POB 97175-615, Birjand, Iran

来源：

NEW JOURNAL OF CHEMISTRY | 2022年 / 47卷 / 01期

关键词：

REDUCED GRAPHENE OXIDE; 1ST-LINE ANTITUBERCULOSIS DRUGS; VOLTAMMETRIC DETERMINATION; CARBON; SENSOR; HEPATOTOXICITY; PYRAZINAMIDE; ETHAMBUTOL; ELECTRODE; NANOCOMPOSITE;

D O I：

10.1039/d2nj04263k

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An ultrasensitive and disposable sensor based on a modified screen-printed carbon electrode (SPCE) was developed for rapid quantification of rifampicin (RIF) and isoniazid (INZ) by differential pulse voltammetry (DPV) in complex media. The surface of the SPCE was simply electrochemically modified with a reduced graphene oxide and nickel hydroxide nanofilm (Ni(OH)(2)@rGO/SPCE) and characterized by atomic force microscopy and cyclic voltammetry. Individual and simultaneous detection of RIF and INZ was accomplished using the Ni(OH)(2)@rGO/SPCE in the ranges of 1.0 x 10(-9)-2.0 x 10(-7) mol L-1 and 2.0 x 10(-7)-5.0 x 10(-5) mol L-1 for RIF and 5.0 x 10(-8)-1.0 x 10(-6) mol L-1 and 1.0 x 10(-6)-1.0 x 10(-4) mol L-1 for INZ with detection limits of 3.0 x 10(-9) mol L-1 and 5.0 x 10(-9) mol L-1, respectively. The developed sensor was successfully applied for the rapid simultaneous determination of analytes in real samples.

引用

页码：500 / 514

页数：15

共 54 条

[1] GO composite encompassing a tetraruthenated cobalt porphyrin-Ni coordination polymer and its behavior as isoniazid BIA sensor [J].

Aguirre-Araque, Juan S. ;

Goncalves, Josue M. ;

Nakamura, Marcelo ;

Rossini, Pamela O. ;

Angnes, Lucio ;

Araki, Koiti ;

Toma, Henrique E. .

ELECTROCHIMICA ACTA, 2019, 300 :113-122

[2] Sensitive electrochemical determination of rifampicin using gold nanoparticles/poly-melamine nanocomposite [J].

Amidi, S. ;

Ardakani, Y. Hosseinzadeh ;

Amiri-Aref, M. ;

Ranjbari, E. ;

Sepehri, Z. ;

Bagheri, H. .

RSC ADVANCES, 2017, 7 (64) :40111-40118

[3]

[Anonymous], 2019, WHO Guidelines on tuberculosis infection prevention and control 2019 Update

[4] Novel electrochemical biosensor based on PVP capped CoFe2O4@CdSe core-shell nanoparticles modified electrode for ultra-trace level determination of rifampicin by square wave adsorptive stripping voltammetry [J].

Asadpour-Zeynali, Karim ;

Mollarasouli, Fariba .

BIOSENSORS & BIOELECTRONICS, 2017, 92 :509-516

[5]

Bloch AB., 1995, MMWR Recomm Rep, V44, P18

[6] Hepatotoxicity in Children Receiving Isoniazid Therapy for Latent Tuberculosis Infection [J].

Chang, Shiow-Huey ;

Nahid, Payam ;

Eitzman, Sarah R. .

JOURNAL OF THE PEDIATRIC INFECTIOUS DISEASES SOCIETY, 2014, 3 (03) :221-227

[7] Simultaneous determination of rifampicin, isoniazid, pyrazinamide and ethambutol in 4-FDC tablet by Raman spectroscopy associated to chemometric approach [J].

Chellini, Paula R. ;

Mendes, Thiago O. ;

Franco, Pedro H. C. ;

Porto, Brenda L. S. ;

Tippavajhala, Vamshi K. ;

Cesar, Isabela C. ;

Oliveira, Marcone A. L. ;

Pianetti, Gerson A. .

VIBRATIONAL SPECTROSCOPY, 2017, 90 :14-20

[8] Development and Validation of an HPLC Method for Simultaneous Determination of Rifampicin, Isoniazid, Pyrazinamide, and Ethambutol Hydrochloride in Pharmaceutical Formulations [J].

Chellini, Paula R. ;

Lages, Eduardo B. ;

Franco, Pedro H. C. ;

Nogueira, Fernando H. A. ;

Cesar, Isabela C. ;

Pianetti, Gerson A. .

JOURNAL OF AOAC INTERNATIONAL, 2015, 98 (05) :1234-1239

[9]

Chokkareddy R., 2019, Sens. Lett., V17, P833, DOI DOI 10.1166/SL.2019.4157

[10] The role of mutators in the emergence of antibiotic-resistant bacteria [J].

Chopra, I ;

O'Neill, AJ ;

Miller, K .

DRUG RESISTANCE UPDATES, 2003, 6 (03) :137-145

← 1 2 3 4 5 6 →