Determination of polycyclic aromatic hydrocarbons in seawater using stir bar sorptive extraction-gas chromatography

被引:0
|
作者
Xu, YA [1 ]
Liu, WM [1 ]
Zhao, JH [1 ]
Guan, YF [1 ]
机构
[1] Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116012, Peoples R China
关键词
stir bar sorptive extraction; thermal desorption; polycyclic aromatic hydrocarbons; sample pretreatment; gas chromatography;
D O I
暂无
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The determination of polycyclic aromatic hydrocarbons (PAHs) in seawater was performed by stir bar sorptive extraction (SBSE)-thermal desorption and gas chromatographic ( GC) analysis. The extraction conditions such as extraction time and addition of salt we're studied. The recoveries of the method were at the range of 33.5% similar to 122.4% for 16 PAHs. The limits of detection were 2.74 similar to 13.5 ng/L, the RSDs of the method were 3.8 similar to 13.1%. The PAHs in real life samples from the beaches of Dalian were determined by using SBSE-GC.
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页码:1401 / 1404
页数:4
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