Synthesis and characterization of poly(methyl methacrylate) polymerized by microwave energy or conventional water bath

被引：15

作者：

Acosta-Torres, L. S. ^{[1
]}

Barcelo-Santana, F. H. ^{[1
]}

Alvarez-Gayosso, C. A. ^{[1
]}

Reyes-Gasga, J. ^{[2
]}

机构：

[1] Univ Nacl Autonoma Mexico, Fac Odontol, Div Estudios Posgrado & Invest, Lab Mat Dentales, Mexico City 04510, DF, Mexico

[2] Univ Nacl Autonoma Mexico, Inst Fis, Mexico City 01000, DF, Mexico

来源：

JOURNAL OF APPLIED POLYMER SCIENCE | 2008年 / 109卷 / 06期

关键词：

suspension polymerization; poly(methyl methacrylate); transverse deflection; molecular weight; particle size;

D O I：

10.1002/app.28569

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

In this work, the influence of three different suspension agents (agar, sodium alginate, and gelatin) in the synthesis of poly(methyl methacrylate) (PMMA) particles is reported. Sodium alginate was the best suspension agent, obtaining characteristics closer to commercial denture base resins. Synthesized particles and two commercial acrylic resins (Acron MC and Lucitone 199) were characterized by light microscopy, scanning electron microscopy, characteristic X-ray energy dispersive spectroscopy, thermogravimetric analysis, and molecular weight measure ments. Mechanical tests (transverse deflection behavior) were done using two heat-polymerizing techniques. The results indicated that both the PMMA particles and the commercial acrylic resins have similar characteristics. (C) 2008 Wiley Periodicals, Inc.

引用

页码：3953 / 3960

页数：8

共 28 条

[1]

[Anonymous], 1975, J AM DENT ASSOC, V90, P451

[2]

ARSHADY R, 1996, DESK REFERENCE FUNCT

[3]

CARUSO F, 2004, COLLOIDS COLLOIDS AS

[4]

Cheremisinoff N. P., 1989, HDB POLYM SCI TECHNO

[5]

Craig RG., 1997, Restorative Dental Materials, V10th

[6] Viscometric study of poly(methyl methacrylate-g-propylene oxide) and respective homopolymers [J].

Delpech, MC ;

Oliveira, CMF .

POLYMER TESTING, 2005, 24 (03) :381-386

[7] Synthesis and characterization of PMMA nanocomposites by suspension and emulsion polymerization [J].

Huang, XY ;

Brittain, WJ .

MACROMOLECULES, 2001, 34 (10) :3255-3260

[8] The effect of length and concentration of glass fibers on the mechanical properties of an injection- and a compression-molded denture base polymer [J].

Karacaer, Ö ;

Polat, TN ;

Tezvergil, A ;

Lassila, LVJ ;

Vallittu, PK .

JOURNAL OF PROSTHETIC DENTISTRY, 2003, 90 (04) :385-393

[9]

Kimura H, 1983, J Osaka Univ Dent Sch, V23, P43

[10] Morphology and properties of denture acrylic resins cured by microwave energy and conventional water bath [J].

Lai, CP ;

Tsai, MH ;

Chen, M ;

Chang, HS ;

Tay, HH .

DENTAL MATERIALS, 2004, 20 (02) :133-141

← 1 2 3 →