Porous solvent-free μ2-bis(salicylidene)propane-1,3-diaminato-bis{[bis( salicylidene)propane-1,3-diaminato]iron(III)}

被引:4
作者
Bakir, M
Dasgupta, TP
Dutta, SK
Ngah, N
Yamin, BM
机构
[1] Univ W Indies, Dept Chem, Kingston 7, Jamaica
[2] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Xray Crystallog Lab, Bangi 43600, Selangor, Malaysia
关键词
D O I
10.1107/S1600536805020611
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, [Fe-2(C17H16N2O2)(3)], was isolated from the reaction between iron(III) perchlorate hydrate and a mixture of 1,3-bis(salicylideneamino) propane and triethylamine in ethanol. Recrystallization from a dichloroethane solution resulted in a porous solvent-free array of molecules. The molecule lies on a special position with twofold symmetry.
引用
收藏
页码:M1464 / M1466
页数:3
相关论文
共 15 条
[1]   The Cambridge Structural Database: a quarter of a million crystal structures and rising [J].
Allen, FH .
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 2002, 58 (3 PART 1) :380-388
[2]   A new class of bridged diiron(III) complex with a Schiff-base bridge: Structure and magnetic properties of Di-N,N'-trimethylene bissalicylidenimine(bis-N,N'-trimethylenebissalicylideniminato)iron(III) [J].
Babu, NKC ;
Nair, BU ;
Ramasami, T ;
Yamasaki, M ;
Shibahara, T .
CHEMISTRY LETTERS, 1997, (10) :975-976
[3]  
ELDERMAN Y, 1991, Z KRISTALLOGR, V196, P309
[4]   CRYSTAL-STRUCTURE OF MU-(N,N'-1,3-PROPYL-DISALICYL-ALDIMINATO)-BIS(N,N-1,3-PROPYL-DISALICYLALDIMINATO)-DI-IRON(III) ETHANOL SOLVATE, (OC6H4CHN)2C3H6(FE(OC6H4CHN)2C3H6)2(C2H5OH) [J].
ELMALI, A ;
ATAKOL, O ;
SVOBODA, I ;
FUESS, H .
ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1993, 203 :271-274
[5]   A CAVEAT - SYNTHESIS AND STRUCTURE OF N,N'-PROPYLENEBIS-(SALICYLIDENEIMINATO)NITRATO[O,O]IRON(III) [J].
FANNING, JC ;
WANG, X ;
KOZIOL, AE ;
PALENIK, GJ .
INORGANICA CHIMICA ACTA, 1995, 232 (1-2) :199-201
[6]   NUCLEARITY AND FORMULATION OF SALPN2- COMPLEXES FORMED FROM M(O2CCH3)2 - RESOLUTION OF LONGSTANDING PROBLEMS BY X-RAY CRYSTALLOGRAPHY [J].
GERLI, A ;
HAGEN, KS ;
MARZILLI, LG .
INORGANIC CHEMISTRY, 1991, 30 (24) :4673-4676
[7]  
Nardelli M., 1995, J APPL CRYSTALLOGR, V28, P659, DOI [10.1107/S0021889895007138, DOI 10.1107/S0021889895007138]
[8]   Novel copper(II) complexes of "short" salen homologues.: Structure and magnetic properties of the tetranuclear complex [Cu2(L2)2]2 [H2L2 = phenyl-N,N′-bis(salicylidene)methanediamine] [J].
Pasini, A ;
Demartin, F ;
Piovesana, O ;
Chiari, B ;
Cinti, A ;
Crispu, O .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 2000, (19) :3467-3472
[9]   Synthesis, structure, and magnetic properties of Mn(salpn)N3, a helical polymer, and Fe(salpn)N3, a ferromagnetically coupled dimer (salpnH2 = N,N′-bis(salicylidene)-1,3-diaminopropane) [J].
Reddy, KR ;
Rajasekharan, MV ;
Tuchagues, JP .
INORGANIC CHEMISTRY, 1998, 37 (23) :5978-5982
[10]  
Sheldrick G.M., 1996, SADABS VERSION 2008