3-Ethyl 5-methyl 4-(2-chlorophenyl)-6-methyl-2-[(2-phthalimidoethoxy) methyl]-1,4-dihydropyridine-3,5-dicarboxylate diethyl ether hemisolvate

被引:0
作者
Liu, HC [1 ]
Feng, YQ [1 ]
机构
[1] Tianjin Univ, Sch Chem Engn & Tecnol, Tianjin 300072, Peoples R China
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2005年 / 61卷
关键词
D O I
10.1107/S1600536805023950
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C28H27ClN2O7 center dot 0.5C(4)H(10)O, was synthesized from ethyl 3-amino-4-[2-( phthalimido)ethoxy] crotonate and methyl 2-(2-chlorobenzylidene) acetoacetate by the Hantzsch reaction. The dihydropyridine ring is not planar, but adopts a boat conformation. The dihedral angle between the phthalimide and 2-chlorophenyl ring planes is 66.0 (3)degrees.
引用
收藏
页码:O3006 / O3007
页数:2
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