Identification of intrinsic hydrogen impurities in ZnO with 1H solid-state nuclear magnetic resonance spectroscopy

被引：17

作者：

Wang, Meng ^{[1
]}

Yu, Guiyun ^{[1
,2
]}

Ji, Wenxu ^{[1
]}

Li, Lei ^{[1
]}

Ding, Weiping ^{[1
]}

Peng, Luming ^{[1
]}

机构：

[1] Nanjing Univ, Sch Chem & Chem Engn, Key Lab Mesoscop Chem MOE, Nanjing 210093, Jiangsu, Peoples R China

[2] Yancheng Inst Technol, Sch Chem & Biol Engn, Yancheng 224051, Peoples R China

来源：

CHEMICAL PHYSICS LETTERS | 2015年 / 627卷

基金：

中国国家自然科学基金;

关键词：

LAYERED DOUBLE HYDROXIDES; ZINC-OXIDE; MAS-NMR; NEUTRON-DIFFRACTION; ZEOLITE HY; BONDS; EPSILON-ZN(OH)(2);

D O I：

10.1016/j.cplett.2015.03.024

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

H-1 solid-state nuclear magnetic resonance (NMR) spectroscopy was used to study intrinsic hydrogen (H) impurities in zinc oxide (ZnO), which play a key role in its n-type conductivity. Two H-1 signals were resolved, and assigned for the first time, to interstitial H species (H-i) and H species substituting for oxygen ions (H-O), with the help from the model compound zinc hydroxide (epsilon-Zn(OH)(2)) and H-1 -> O-17 double resonance NMR spectroscopy. (C) 2015 Elsevier B.V. All rights reserved.

引用

页码：7 / 12

页数：6

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