Microwave-assisted polyol synthesis of nanoscale SnSx(x=1,2) flakes

被引:92
作者
Chen, D
Shen, GZ
Tang, KB
Lei, SJ
Zheng, HG
Qian, YT
机构
[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Peoples R China
[2] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Peoples R China
基金
中国国家自然科学基金;
关键词
growth from solutions; nanomaterials; semiconducting materials;
D O I
10.1016/j.jcrysgro.2003.09.009
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The tin sulfides compounds SnS and SnS2 nanoflakes were prepared by the microwave-assisted polyol synthetic method. The as-prepared nanoscale flakes were characterized by X-ray powder diffraction, transmission electron microscopy, selected area electron diffraction, X-ray photoelectron spectroscopy and Raman spectra. The influences of solvents and microwave irradiation on the formation of products have been studied. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:469 / 474
页数:6
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