Analysis of main pigments and other ingredients in lac color product

被引:7
作者
Hirata, K [1 ]
Uematsu, Y [1 ]
Suzuki, K [1 ]
Iida, K [1 ]
Yasuda, K [1 ]
Saito, K [1 ]
机构
[1] Tokyo Metropolitan Res Lab Publ Hlth, Shinjuku Ku, Tokyo 1690073, Japan
来源
JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN | 2001年 / 42卷 / 02期
关键词
lac color product; laccaic acids; HPLC HPLC/PDA; electrospray ionization mass spectrometry;
D O I
10.3358/shokueishi.42.109
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
The contents of the main pigments and other ingredients in commercial lac color products were determined by HPLC using an RP-18 column with 0.1 mol/L citric acid buffer solution-methanol (16 : 5) as the mobile phase, and a photodiode array (PDA) detector set at 280 nm and 490 nm. The main pigments were confirmed by PDA and electrospray ionization mass spectrometry. Laccaic acids A, B, C and E were detected in all lac color products, and the ratio of content of laccaic acid A in all products was over 50%. The total contents of laccaic acids A, B and C in lac color food additive products and reagent products were 775 similar to 858, 797 and 779 g/kg, respectively. As for the contents of ingredients except pigments in commercial food additive products, the maximum moisture content was about 10%, and ether-soluble substances amounted to 0.5 similar to3.6%.
引用
收藏
页码:109 / 113
页数:5
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