The reliability in flexural strength testing of a novel dental composite

被引:46
作者
Palin, WM
Fleming, GJP
Burke, JFT
Marquis, PM
Randall, RC
机构
[1] Univ Birmingham, Sch Dent, Biomat Unit, Birmingham B4 6NN, W Midlands, England
[2] Univ Birmingham, Sch Dent, Primary Dent Care Unit, Birmingham B4 6NN, W Midlands, England
[3] 3M Co, ESPE, St Paul, MN 55144 USA
关键词
dental composite; oxirane monomers; cationic polymerisation; bi-axial flexure; three-point flexure; Weibull statistics;
D O I
10.1016/S0300-5712(03)00110-6
中图分类号
R78 [口腔科学];
学科分类号
1003 ;
摘要
Objectives. To investigate the reliability of bi-axial flexure and three-point flexure testing of an experimental, low-shrink oxirane-based dental composite, EXL596 compared with two conventional methacrylate based restoratives, Z250 and Z100. Methods. Specimens (n = 20) of a novel. oxirane-based composite and two commercially available methacrylate based composites were fabricated for flexural testing to evaluate mean bi-axial flexure strengths, three-point flexure strengths and the associated Weibull moduli (m) following 24 h immersion in a lightproof waterbath maintained at 37 +/- 1 degreesC. Results. Mean bi-axial, flexure strengths and the associated m of EXL596, Z250 and Z100 were 168 +/- 11 MPa (m = 16.2 +/- 4), 140 +/- 12 MPa (m = 11.9 +/- 3) and 126 +/- 13 MPa (m = 10.2 +/- 2), respectively. Three-point flexure strengths and the associated m of EXL596, Z250 and Z100 were 113 +/- 15 MPa (m = 9.2 +/- 2), 92 +/- 10 MPa (m = 8.5 +/- 2) and 79 +/- 16 MPa (m = 6.3 +/- 1), respectively. Conclusions. The present investigation suggests that bi-axial. flexure strength testing of dental resin-based composites provides a more reliable testing method than three-point flexure. The increased reliability was considered in terms of the associated Weibull. moduli following bi-axial flexure testing as a result of the elimination of the additional induced variability introduced during the curing regime of three-point flexure specimens. (C) 2003 Elsevier Ltd. All rights reserved.
引用
收藏
页码:549 / 557
页数:9
相关论文
共 38 条
[1]   Photopolymerization kinetics of multifunctional monomers [J].
Andrzejewska, E .
PROGRESS IN POLYMER SCIENCE, 2001, 26 (04) :605-665
[2]   Influence of UEDMA, BisGMA and TEGDMA on selected mechanical properties of experimental resin composites [J].
Asmussen, E ;
Peutzfeldt, A .
DENTAL MATERIALS, 1998, 14 (01) :51-56
[3]   Effect of irradiation time on tensile properties of stiffness and strength of composites [J].
Baharav, H ;
Brosh, T ;
Pilo, R ;
Cardash, H .
JOURNAL OF PROSTHETIC DENTISTRY, 1997, 77 (05) :471-474
[4]   INFLUENCE OF TEST METHOD ON FAILURE STRESS OF BRITTLE DENTAL MATERIALS [J].
BAN, S ;
ANUSAVICE, KJ .
JOURNAL OF DENTAL RESEARCH, 1990, 69 (12) :1791-1799
[5]   MEASUREMENT OF THE TENSILE STRENGTH OF BRITTLE MATERIALS [J].
BERENBAUM, R ;
BRODIE, I .
BRITISH JOURNAL OF APPLIED PHYSICS, 1959, 10 (06) :281-287
[6]   Analysis of strength properties of light-cured resin composites [J].
Brosh, T ;
Ganor, Y ;
Belov, I ;
Pilo, R .
DENTAL MATERIALS, 1999, 15 (03) :174-179
[7]  
Craig RG., 1993, RESTORATIVE DENT MAT, V9th
[8]  
DARVELL BW, 1990, J MATER SCI, V25, P757
[9]  
Davies D.G.S., 1973, P BRIT CERAMIC SOC, V22, P429
[10]  
DEWITH G, 1989, J AM CERAM SOC, V72, P1538, DOI 10.1111/j.1151-2916.1989.tb07702.x